Preparation of monodispersed α-Fe2O3 nanoparticles by a hydrothermal synthetic route

被引:7
|
作者
Wang, Hong [1 ]
Geng, Wang-Chang [2 ]
机构
[1] Sichuan Univ Sci & Engn, Dept Mat & Chem Engn, Zigong 643000, Peoples R China
[2] Northwestern Polytech Univ, Dept Appl Chem, Sch Sci, Xian 710129, Peoples R China
关键词
alpha-Fe2O3; Monodisperse; Magnetic properties; MAGNETIC-PROPERTIES; PARTICLES; UNIFORM; GROWTH;
D O I
10.1007/s11164-011-0280-4
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Monodispersed alpha-Fe2O3 nanoparticles modified by sodium dodecylbenzene sulfonate (SDBS) surfactant and assisted by glycerol have been successfully synthesized via a hydrothermal process using FeCl3 center dot 6H(2)O as the starting precursor. These nanoparticles possess good crystallinity and have an average particle size of 100 nm. The as-prepared products are characterized by X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, and a superconducting quantum interference device magnetometer. SDBS and glycerol played an important role in controlling the final morphology of the products. Magnetic hysteresis measurements reveal that monodispersed alpha-Fe2O3 nanoparticles exhibit normal ferromagnetic behaviors with the remanent magnetization and coercivity of 0.2389 emu/g and 2339.0 Oe at room temperature.
引用
收藏
页码:523 / 529
页数:7
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