3D visualization of dislocation arrangement using scanning electron microscope serial sectioning method

被引：19

作者：

Yamasaki, S. ^{[1
]}

Mitsuhara, M. ^{[1
]}

Ikeda, K. ^{[1
]}

Hata, S. ^{[1
]}

Nakashima, H. ^{[1
]}

机构：

[1] Kyushu Univ, Fac Engn Sci, Kasuga, Fukuoka 8168580, Japan

来源：

SCRIPTA MATERIALIA | 2015年 / 101卷

基金：

日本学术振兴会;

关键词：

Dislocation; 3D reconstruction; Scanning electron microscopy (SEM); Electron channeling contrast imaging (ECCI); Nickel alloys; CHANNELING CONTRAST; BULK MATERIALS; ALLOY; 617; TOMOGRAPHY; MICROSTRUCTURE; SILICON;

D O I：

10.1016/j.scriptamat.2015.02.001

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

We performed the three-dimensional visualization of dislocations through serial sectioning and use of SEM electron channeling contrast (ECC) images for a crept nickel-based alloy. We successfully reconstructed a volume of approximately 7.5 mu m(3), including dislocation arrangements, by performing calculations based on the continuous tomograms of ECC images. By incorporating the information on crystal orientation obtained by the electron back-scattered diffraction, we verified that the three-dimensional arrangement of dislocations, such as slip plane, was accurately reflected in the three-dimensional volume. (C) 2015 Acta Materialia Inc. Published by Elsevier Ltd.

引用

页码：80 / 83

页数：4

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