Polyaniline (PANI) was grafted covalently onto the surfaces of the phenylaminopropyl silica nanoparticles (PASNs) by the in-situ chemical oxidation of aniline with ammonium peroxydisulfate (APS) using a dispersion polymerization method. A percentage of grafting (PG%) of 234.0% and a grafting efficiency (GE%) of 54.1% were achieved, calculated from the results of elemental analysis (EA). The polyaniline grafted silica nanoparticles (PANI-SNs) were also characterized by FT-IR, UV/vis, TEM, XPS and TGA. The four probe conductivities were also measured.
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Kyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Ragupathy, D.
Gopalan, A.
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Kyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Kyungpook Natl Univ, Dept Nanosci & Technol, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Gopalan, A.
Kim, Kyeong-Wung
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Kyungpook Natl Univ, Dept Nanosci & Technol, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Kim, Kyeong-Wung
Lee, Kwang Pill
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Kyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea
Kyungpook Natl Univ, Dept Nanosci & Technol, Taegu 702701, South KoreaKyungpook Natl Univ, Dept Chem, Grad Sch, Taegu 702701, South Korea