Synthesis and Characterization of Nano-γ-Fe2O3 by Sol-Gel Method

被引：0

作者：

Huang, Jian ^{[1
]}

Gong, Zhuqing ^{[2
]}

Yang, Xiyun ^{[2
]}

机构：

[1] Cent S Univ, Coll Chem & Chem Engn, Changsha 410083, Peoples R China

[2] Cent S Univ, Coll Met Sci & Engn, Changsha 410083, Peoples R China

来源：

ADVANCED SCIENCE LETTERS | 2011年 / 4卷 / 11-12期

基金：

中国国家自然科学基金;

关键词：

Nano-gamma-Fe2O3; Sol-Gel; Ferric Citrate; Magnetic Material; DUAL-COLOR HYBRIDIZATION; IRON-OXIDE NANOPARTICLES; SINGLE-BASE EXTENSION; MAGNETIC NANOPARTICLES; GAMMA-FE2O3; NANOPARTICLES; IMMUNOLOGICAL METHOD; ARRAY; FABRICATION; SURFACE; ROUTE;

D O I：

10.1166/asl.2011.1864

中图分类号：

O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];

学科分类号：

07 ; 0710 ; 09 ;

摘要：

The synthesis and characterization of nano-gamma-Fe2O3 was described by sol-gel method. The optimal conditions for the formation of iron citric acid sol-gel were that the concentration of ferrite citrate was 0.8 mol/L, the pH was 7 and the reaction temperature was 40 degrees C. DTA, XRD, FT-IR, and TEM analysis were employed to characterize the properties of the as-prepared gamma-Fe2O3. TG-DTA, XRD and FT-IR characterization indicate that the appropriate temperature for the formation of gamma-Fe2O3 by Sol-gel method is 450 degrees C and the particle size of gamma-Fe2O3 formed is about 32 nm by the Scherrer formula and TEM under the optimal conditions.

引用

页码：3662 / 3665

页数：4

共 50 条

[1] Synthesis and Characterization of Fe2O3 Prepared Via Sol-Gel Method
Rahman, Noor Azreen Abdul
Mustaffa, Nur Amalina
Aziz, Nor Diyana Abdul
Bader, Nurhanna
Kannarulzaman, Norlida
[J]. ADVANCEMENT OF MATERIALS AND NANOTECHNOLOGY II, 2012, 545 : 410 - 413
[2] Sol-gel synthesis and characterization of α-Fe2O3 nanoparticles
Raja, K.
Jaculine, M. Mary
Jose, M.
Verma, Sunil
Prince, A. A. M.
Ilangovan, K.
Sethusankar, K.
Das, S. Jerome
[J]. SUPERLATTICES AND MICROSTRUCTURES, 2015, 86 : 306 - 312
[3] Preparation and characterization of α-FeOOH and α-Fe2O3 by sol-gel method
Dar, MA
Kulkarni, SK
Ansari, ZA
Ansari, SG
Shin, HS
[J]. JOURNAL OF MATERIALS SCIENCE, 2005, 40 (11) : 3031 - 3034
[4] Synthesis, characterization and magnetic properties of ε-Fe2O3 nanoparticles prepared by sol-gel method
Khan, Irfan
Morishita, Sakura
Higashinaka, Ryuji
Matsuda, Tatsuma D.
Aoki, Yuji
Kuzmann, Erno
Homonnay, Zoltan
Katalin, Sinko
Pavic, Luka
Kubuki, Shiro
[J]. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2021, 538
[5] Growth of nano-α-Fe2O3 in a titania matrix by the sol gel route
Kundu, TK
Mukherjee, M
Chakravorty, D
Sinha, TP
[J]. JOURNAL OF MATERIALS SCIENCE, 1998, 33 (07) : 1759 - 1763
[6] Growth of nano-α-Fe2O3 in a titania matrix by the sol–gel route
T. K Kundu
M Mukherjee
D Chakravorty
T. P Sinha
[J]. Journal of Materials Science, 1998, 33 : 1759 - 1763
[7] Sol-gel mediated synthesis of Fe2O3 nanorods
Woo, K
Lee, HJ
Ahn, JP
Park, YS
[J]. ADVANCED MATERIALS, 2003, 15 (20) : 1761 - +
[8] Nanometric particle size and phase controlled synthesis and characterization of γ-Fe2O3 or (α plus γ)-Fe2O3 by a modified sol-gel method
Silva, Marcela F.
de Oliveira, Luiz A. S.
Ciciliati, Mariani A.
Silva, Lais T.
Pereira, Bruna S.
Hechenleitner, Ana Adelina W.
Oliveira, Daniela M. F.
Pirota, Kleber R.
Ivashita, Flavio F.
Paesano, Andrea, Jr.
Martin Pastor, J.
Inaki Perez-Landazabal, J.
Pineda, Edgardo A. G.
[J]. JOURNAL OF APPLIED PHYSICS, 2013, 114 (10)
[9] Synthesis and characterization of Y2O3/Fe2O3/TiO2 nanoparticles by sol-gel method
Ismail, AA
[J]. APPLIED CATALYSIS B-ENVIRONMENTAL, 2005, 58 (1-2) : 115 - 121
[10] Spectroellipsometric Characterization of Multilayer Sol-Gel Fe2O3 Films
Mariuca Gartner
Maria Crisan
A. Jitianu
R. Scurtu
Raluca Gavrila
Isabella Oprea
Maria Zaharescu
[J]. Journal of Sol-Gel Science and Technology, 2003, 26 : 745 - 748

← 1 2 3 4 5 →