One-pot multi-component synthesis of polyhydroquinolines at ambient temperature

被引：50
|
作者：
Undale, K. A. [1 ]
Shaikh, T. S. [1 ]
Gaikwad, D. S. [1 ]
Pore, D. M. [1 ]
机构：
[1] Shivaji Univ, Dept Chem, Kolhapur 416004, Maharashtra, India
来源：
COMPTES RENDUS CHIMIE | 2011年 / 14卷 / 05期
关键词：
Multi-component; Polyhydroquinolines; Hantzsch condensation; One-pot synthesis; SOLVENT-FREE CONDITIONS; LIQUID-PHASE SYNTHESIS; SILICA SULFURIC-ACID; HANTZSCH REACTION; MICROWAVE IRRADIATION; CALCIUM-ANTAGONISM; ROOM-TEMPERATURE; DERIVATIVES; CATALYST; 1,4-DIHYDROPYRIDINES;
D O I：
10.1016/j.crci.2010.09.009
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An efficient and eco-friendly one-pot synthesis of polyhydroquinolines at ambient temperature from the multi-component reaction of aldehyde, 1,3-diketone, beta-keto ester and ammonium acetate in ethanol medium is described. The probable mechanism of transformation is suggested. The features of this procedure are mild reaction conditions, no need of external catalyst, good yields and the operational simplicity at ambient temperature. (C) 2010 Academie des sciences. Published by Elsevier Masson SAS. All rights reserved.
引用
收藏
页码：511 / 515
页数：5
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