Synthesis, Structure and Characterization of a Novel Two-Dimensional Supramolecular Mn(II) Coordination Polymer Constructed from a 1,10-Phenanthroline Derivative and a Flexible Dicarboxylate

被引：17
|
作者：
Kong, Zhi-Guo [1 ]
Ma, Xiao-Yuan [1 ]
Xu, Zhan-Lin [1 ]
机构：
[1] Jilin Normal Univ, Dept Chem, Siping 136000, Peoples R China
来源：
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES | 2010年 / 65卷 / 09期
关键词：
Coordination Polymer; Crystal Structure; Glutaric Acid; 1 10 Phenanthroline Derivative; LIGANDS;
D O I：
10.1515/znb-2010-0920
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The title complex, [Mn-2(glu)(L)(2)(HL)(2)] 0 5H(2)O (H(2)glu = glutaric acid HL = 2 (2 chloro-6-fluorophenyl)-1H imidazo[4 5-f] [1 10]phenanthroline) has been synthesized using a hydrothermal method and characterized by elemental analysis IR spectroscopy and single-crystal X-ray diffraction Crystal data C162H88Cl8F8Mn4N32O9, triclinic space group P (1) over bar, a = 14 932(5) b = 16 414(5) c = 17 891(5) A alpha = 115 851(5) beta = 91 288(5) gamma = 112894(5)degrees, V = 3536 4(19) A(3) Z = 1 Compound 1 exhibits 1D chains which are further stacked by C-H pi interactions to give two dimensional supramolecular layers
引用
收藏
页码：1173 / 1176
页数：4
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