Solvent-free synthesis of metal phosphate-oxalates with layered and zeolitic structures

被引：4

作者：

Luan, Lindong ^{[1
]}

Zou, Guohong ^{[2
]}

Lin, Zhien ^{[2
]}

Cai, Huaqiang ^{[1
]}

Huang, Hui ^{[1
]}

机构：

[1] China Acad Engn Phys, Inst Chem Mat, Mianyang 621900, Peoples R China

[2] Sichuan Univ, Coll Chem, Chengdu 610064, Sichuan, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2018年 / 96卷

基金：

中国国家自然科学基金;

关键词：

Solvent-free synthesis; Metal phosphate-oxalate; Zeolitic topology; Magnetism; Photoluminescence; SULFATE-OXALATES; BIMODAL POROSITY; ZINC PHOSPHATE; LIGHT PHOSPHOR; FRAMEWORK; TOPOLOGIES; CLUSTER; IONS; UNIT;

D O I：

10.1016/j.inoche.2018.08.003

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Three new metal phosphate-oxalates, namely, (H(2)dmp)(0.5)center dot Mn(H2PO4)(C2O4) (1), and H2R center dot In-2(HPO4)(2)(H2PO4)(2)(C2O4)center dot H2O (R = dmp (2) and dmapa (3)) were prepared under solvent-free conditions, where dmp = 1,4-dimethylpiperazine and dmapa = 3-(dimethylamino)-1-propylamine. Compound 1 has a layered structure with an sql net. Compounds 2 and 3 are isostructural and have large 16-ring channels with a zeolitic crb net. The temperature dependence of the magnetic susceptibility of compound 1 and the photoluminescent property of compound 3 were investigated.

引用

页码：65 / 68

页数：4

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