Direct structure elucidation by powder X-ray diffraction of a metal-organic framework material prepared by solvent-free grinding

被引：89

作者：

Fujii, Kotaro ^{[2
]}

Garay, Ana Lazuen ^{[1
]}

Hill, Janeen ^{[1
]}

Sbircea, Elena ^{[1
]}

Pan, Zhigang ^{[2
]}

Xu, Mingcan ^{[2
]}

Apperley, David C. ^{[3
]}

James, Stuart L. ^{[1
]}

Harris, Kenneth D. M. ^{[2
]}

机构：

[1] Queens Univ Belfast, Sch Chem & Chem Engn, CenTACat, Belfast BT9 5AG, Antrim, North Ireland

[2] Cardiff Univ, Sch Chem, Cardiff CF10 3AT, S Glam, Wales

[3] Univ Durham, Dept Chem, Durham DH1 3LE, England

来源：

CHEMICAL COMMUNICATIONS | 2010年 / 46卷 / 40期

基金：

英国工程与自然科学研究理事会;

关键词：

INITIO STRUCTURE DETERMINATION; CRYSTAL-STRUCTURE SOLUTION; GENETIC ALGORITHM; MECHANOCHEMICAL PREPARATION; DEHYDRATION PROCESS; MOLECULAR MATERIALS; COORDINATION; PHASE; REACTIVITY; 1D;

D O I：

10.1039/c0cc02635b

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Powder X-ray diffraction (XRD) has been exploited to establish the structural properties of a porous interpenetrated mixed-ligand metal-organic framework material prepared by solid-state grinding, recognizing that product phases from mechanochemical synthesis are typically microcrystalline powders. The importance of subjecting the powder XRD data to rigorous scrutiny in such applications is emphasized.

引用

页码：7572 / 7574

页数：3

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