Preparation of Barium Sulfate Nanoparticles Using Semi-Batch Precipitation

被引:0
|
作者
Berenjian, A. [2 ]
Ghasemi, M. R. [2 ]
Zarghi, A. [1 ]
机构
[1] Shahid Beheshti Univ MC, Dept Pharmaceut Chem, Tehran, Iran
[2] Azad Univ, N Tehran Branch, Dept Chem Engn, Tehran, Iran
关键词
Barium sulfate; Nanoparticles; Precipitation reaction; CALCIUM-CARBONATE PARTICLES; BASO4; NANOPARTICLES; REACTOR; MICROEMULSIONS; SIZE;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The present work aims at the investigation of different aspects on the production of barium sulfate nanoparticles. The influence of different process control parameters such as the feeding rate, temperature and initial concentrations of the reactants on the particle size has been studied to gain a deeper understanding of the important controlling mechanisms in the formation of BaSO4 nanoparticles. The experiments were carried out via a simple Precipitation reaction of sodium sulfate with barium chloride in a semi-batch reactor. Present results showed that the reaction temperature, molar ratio of Ba2+-SO42- (R) and presence of ethanol were the most important parameters for the size control of barium sulfate particles.
引用
收藏
页码:491 / 494
页数:4
相关论文
共 50 条
  • [31] CALCULATIONS ON ISOTHERMAL SEMI-BATCH REACTORS
    HUGO, P
    [J]. CHEMIE INGENIEUR TECHNIK, 1981, 53 (02) : 107 - 109
  • [32] Modeling of batch and semi-batch membrane filtration processes
    Kovacs, Z.
    Discacciati, M.
    Samhaber, W.
    [J]. JOURNAL OF MEMBRANE SCIENCE, 2009, 327 (1-2) : 164 - 173
  • [33] Monitoring Semi-Batch Reactor using Principal Component Analysis
    Damarla, S. K.
    Kundu, M.
    [J]. 2012 INTERNATIONAL CONFERENCE ON EMERGING TRENDS IN ELECTRICAL ENGINEERING AND ENERGY MANAGEMENT (ICETEEEM - 2012), 2012, : 6 - 10
  • [34] Thermal explosion in semi-batch reactors
    N. G. Samoilenko
    B. L. Korsunskii
    Yu. N. Finaeva
    L. V. Kustova
    [J]. Combustion, Explosion, and Shock Waves, 2014, 50 : 412 - 416
  • [35] Intensifying micromixing in a semi-batch reactor using a Rushton turbine
    Assirelli, M
    Bujalski, W
    Eaglesham, A
    Nienow, AW
    [J]. CHEMICAL ENGINEERING SCIENCE, 2005, 60 (8-9) : 2333 - 2339
  • [36] Thermal explosion in semi-batch reactors
    Samoilenko, N. G.
    Korsunskii, B. L.
    Finaeva, Yu. N.
    Kustova, L. V.
    [J]. COMBUSTION EXPLOSION AND SHOCK WAVES, 2014, 50 (04) : 412 - 416
  • [37] TEMPERATURE CONTROL IN SEMI-BATCH REACTORS
    DOUGHERTY, EP
    WESTKAEMPER, PH
    WU, RS
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1988, 195 : 148 - PMSE
  • [38] A dynamic model for process flowsheet simulation of semi-batch precipitation of sparingly soluble salts
    Rehage, Hendrik
    Semmel, Malte
    Kind, Matthias
    [J]. COMPUTERS & CHEMICAL ENGINEERING, 2020, 137
  • [39] Calcium deficient hydroxyapatite by precipitation: Continuous process by vortex reactor and semi-batch synthesis
    Gecim, Gozde
    Donmez, Sinan
    Erkoc, Ertugrul
    [J]. CERAMICS INTERNATIONAL, 2021, 47 (02) : 1917 - 1928
  • [40] Optimisation of a semi-batch chromatographic reactor
    West, CM
    Smith, EL
    [J]. 1996 ICHEME RESEARCH EVENT - SECOND EUROPEAN CONFERENCE FOR YOUNG RESEARCHERS IN CHEMICAL ENGINEERING, VOLS 1 AND 2, 1996, : 148 - 150