The effect of magnetic annealing on crystallographic texture and magnetic properties of Fe-2.6% Si

被引:9
|
作者
Salih, M. Z. [1 ]
Uhlarz, M.
Pyczak, F. [2 ,3 ]
Brokmeier, H. -G. [1 ,2 ,3 ]
Weidenfeller, B. [4 ]
Al-Hamdany, N. [1 ]
Gan, W. M. [2 ,3 ]
Zhong, Z. Y. [1 ]
Schell, N. [2 ,3 ]
机构
[1] Tech Univ Clausthal, Inst Werkstoffkunde & Werkstofftech, D-38678 Clausthal Zellerfeld, Germany
[2] Helmholtz Zentrum Dresden Rossendorf, Dresden High Magnet Field Lab HLD, D-01328 Dresden, Germany
[3] Helmholtz Zentrum Geesthacht, Inst Mat Res, D-21502 Geesthacht, Germany
[4] Abteilung Mat Wissensch, Inst Elektrochem, D-38678 Clausthal Zellerfeld, Germany
关键词
Electric steel; Hot rolling; Cold rolling; Defects density; Magnetic annealing; Magnetic properties; Neutron diffraction; X-RAY; NEUTRON-DIFFRACTION; RECRYSTALLIZATION; DIFFRACTOMETER; CONTRAST; FIELD;
D O I
10.1016/j.jmmm.2015.01.004
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The effect of magnetic annealing on crystallographic texture, microstructure, defects density and magnetic properties of a Fe-2.6% Si steel has been analyzed. After two stage cold rolling (75% and 60% cold rolled) with intermediate annealing process at (600 degrees C/1 h) the sample annealed at 600 degrees C for one hour during which different magnetic field of 0, 7 and 14T were applied has been investigated. The effect of defects density after cold rolling process on the recrystallization texture and magnetic properties was characterized. Heat treatments under a high external field of 14 T show a drastic improvement of the magnetic properties such as significantly increased permeability. Neutron diffraction measurements were preferred for measurement of the bulk sample texture so that sufficient grain statistics were obtained. Because of its small wavelength (0.05-0.2 angstrom) Synchrotron diffraction with high photon energy was used to evaluate the defects density by a modified Williamson-Hall plot. (C) 2015 Published by Elsevier B.V.
引用
收藏
页码:350 / 359
页数:10
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