A neutral chiral diamond-like 3D zinc(II) coordination network with sulfasalazine

被引：8
|
作者：
Chen, Zhen-Feng [1 ]
Shu Kang [1 ]
Shi, Shao-Ming [2 ]
Abrahams, Brendan F. [2 ]
Hong Liang [1 ]
机构：
[1] Guangxi Normal Univ, Sch Chem & Chem Engn, Key Lab Med Chem Resources & Mol Engn, Minist Educ, Guilin 541004, Peoples R China
[2] Univ Melbourne, Sch Chem, Melbourne, Vic 3010, Australia
来源：
JOURNAL OF MOLECULAR STRUCTURE | 2008年 / 882卷 / 1-3期
基金：
中国国家自然科学基金;
关键词：
sulfasalazine; zinc(II); chiral; crystal structure;
D O I：
10.1016/j.molstruc.2007.09.026
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A neutral chiral diamond-like 3D zinc(II) coordination network with sulfasalazine, [Zn(H-2-Sulf)mu-OH](n) (H-3-Sulf = sulfasalazine) (1), was synthesized by the hydrothermal reaction of sulfasalazine and Zn(OAc)(2)center dot H2O or Zn(OH)(2). X-ray diffraction study shows that 1 crystallizes n the orthorhombic system, P2(1)2(1)2(1) space group, a = 5.2730(5), b = 17.8473(17), c = 20.319(2) angstrom, V = 1912.2(3) angstrom(3), Z = 4, D-c = 1.660 g(-3). In 1, the Zn centers are linked by inequivalent ligand bridges, OH- and deprotonated sulfasalazine. Individual crystals are chiral however the product consists of a racemic mixture of crystals. (C) 2008 Published by Elsevier B.V.
引用
收藏
页码：134 / 139
页数：6
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