Enantiomerically pure cage-shaped (1S,4S,5R)-4-hydroxy-2,6-diazabicyclo[3.3.0]octane and (1S,4R,5R)-4-hydroxy-2-oxa-6-azabicyclo[3.3.0]octane: Synthesis and test for enantioselective catalysis

被引:3
|
作者
Lin, GQ
Shi, ZC
机构
[1] Shanghai Inst. of Organic Chemistry, Chinese Academy of Sciences, 354 Fenglin Rd., 200032, Shanghai
基金
中国国家自然科学基金;
关键词
D O I
10.1016/S0040-4020(96)01049-6
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A synthesis of cage-shaped compounds-(IS,4S,5R)-4-hydroxy-2,6-diazabicyclo[3.3.0]octane and (IS,4R,SR)-4-hydroxy-2-oxa-6-azabicyclo[3.3.0]octane described. The test for enantioselective catalysis also reported. (C) 1997, Elsevier Science Ltd.
引用
收藏
页码:1369 / 1382
页数:14
相关论文
共 50 条
  • [21] SYNTHESIS OF(4S,5R)-5-HYDROXY-4-DECANOLIDE.THE PROPOSED AUTOREGULATOR FROM STREPTOMYCES
    Da Qing SUN Ke Qian CHEN Department of Chemistry Suzhou University
    ChineseChemicalLetters, 1990, (03) : 207 - 208
  • [22] OPTIMIZATION OF PRODUCTION CONDITIONS FOR 4-HYDROXY-2,6-DIOXABICYCLO(3,3,0)OCTAN-8-ONE[1S,4S,5R] BY CATALYTIC-OXIDATION
    JACQUET, F
    RIGAL, L
    GASET, A
    JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY, 1990, 48 (04) : 493 - 506
  • [23] Synthesis of terminal alkynes based on (1S,3R,4R)- and (1S,3S,4R)-2-azabicyclo[2.2.1]heptane
    Steppeler, Franz
    Gorecki, Marcin
    Wojaczynska, Elzbieta
    ARKIVOC, 2021, : 25 - 36
  • [24] THE CATALYTIC-OXIDATION OF 4,8-DIHYDROXY-2,6-DIOXABICYCLO (3.3.0) OCTANE [1R,4S,5R,8R] ON PLATINUM IN THE PRESENCE OF OXYGEN - A STUDY OF THE INFLUENCE OF THE MAJOR PARAMETERS
    JACQUET, F
    GRANADO, C
    RIGAL, L
    GASET, A
    APPLIED CATALYSIS, 1985, 18 (01): : 157 - 172
  • [25] (3S,4S,5R)-3-hydroxy-4-methyl-5-vinyltetrahydropyran-2-one
    Koerner, Marleen
    Schuermann, Markus
    Preut, Hans
    Hiersemann, M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3012 - U3245
  • [26] A Convenient Approach to the Enantiopure (1S,2S,4S,5S)-and (1R,2S,4R,5S)-2,5-Bis(phenylmethyl)-1,4-diazabicyclo[2.2.2]-octane
    邱丽华
    沈宗旋
    陈五红
    张勇
    张雅文
    ChineseJournalofChemistry, 2003, (08) : 1098 - 1100
  • [27] An efficient synthesis of enantiomerically pure (1R,2S,5S)- and (1S,2R,5R)-rosaprostol methyl esters
    Murcia, M. Carmen
    de la Herran, Gabriela
    Plumet, Joaquin
    Csaky, Aurelio G.
    SYNLETT, 2007, (10) : 1553 - 1556
  • [28] First Stereoselective Synthesis of (1R,2R,4R)- and (1S,2R,4S)-2-Substituted-1-azabicyclo[2.2.1]heptanes
    Etayo, Pablo
    Badorrey, Ramon
    Diaz-de-Villegas, Maria D.
    Galvez, Jose A.
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 2009 (09) : 1372 - 1376
  • [29] SYNTHESIS OF (1S 2R 4R 5S 6R)-1,2,4,5,6-PENTA-O-BENZOYLMYOINOSITOL
    MERCIER, D
    GERO, SD
    TETRAHEDRON LETTERS, 1968, (31) : 3459 - &
  • [30] Synthesis and Crystal Structure of Unexpected (1S,4R,5R,6S)-4-Cyano-2,2,6-trimethyl-3-azabicyclo[3.3.1]nonan-6-yl Acetate
    Williams, Steven Gareth
    Bhadbhade, Mohan
    Bishop, Roger
    Ung, Alison Thavary
    AUSTRALIAN JOURNAL OF CHEMISTRY, 2017, 70 (12) : 1269 - 1273