Efficient Catalytic Synthesis of α,ω-Di(spiro[adamantane-2,3′-[1,2,4,5,7]tetroxazocan]-7′-yl)alkanes

被引：3

作者：

Makhmudiyarova, N. N. ^{[1
]}

Koroleva, L. S. ^{[2
]}

Meshcheryakova, E. S. ^{[1
]}

Ibragimov, A. G. ^{[1
]}

机构：

[1] Russian Acad Sci, Inst Petrochem & Catalysis, Ufa 450075, Russia

[2] Bashkir State Univ, Ufa 450076, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2020年 / 56卷 / 03期

基金：

俄罗斯科学基金会;

关键词：

catalysis; recyclization; alpha; omega-diaminoalkanes; spiro[adamantane-2,3 '-[1,2,4,5,7]pentoxocane; spiro[adamantane-2,3 '-[1,2,4,5,7]tetroxazocanes; X-ray analysis; EPOXIDATION;

D O I：

10.1134/S1070428020030021

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

An efficient method has been developed for the synthesis of alpha,omega-di(spiro[adamantane-2,3'-[1,2, 4,5,7]tetroxazocan]-7'-yl)alkanes by recyclization of spiro[adamantane-2,3'-[1,2,4,5,7]pentoxocane] with alpha,omega-diaminoalkanes in THF in the presence of Sm(NO3)(3)center dot 6 H2O as catalyst.

引用

页码：378 / 384

页数：7

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