Efficient Catalytic Synthesis of α,ω-Di(spiro[adamantane-2,3′-[1,2,4,5,7]tetroxazocan]-7′-yl)alkanes

被引：3
|
作者：
Makhmudiyarova, N. N. [1 ]
Koroleva, L. S. [2 ]
Meshcheryakova, E. S. [1 ]
Ibragimov, A. G. [1 ]
机构：
[1] Russian Acad Sci, Inst Petrochem & Catalysis, Ufa 450075, Russia
[2] Bashkir State Univ, Ufa 450076, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2020年 / 56卷 / 03期
基金：
俄罗斯科学基金会;
关键词：
catalysis; recyclization; alpha; omega-diaminoalkanes; spiro[adamantane-2,3 '-[1,2,4,5,7]pentoxocane; spiro[adamantane-2,3 '-[1,2,4,5,7]tetroxazocanes; X-ray analysis; EPOXIDATION;
D O I：
10.1134/S1070428020030021
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An efficient method has been developed for the synthesis of alpha,omega-di(spiro[adamantane-2,3'-[1,2, 4,5,7]tetroxazocan]-7'-yl)alkanes by recyclization of spiro[adamantane-2,3'-[1,2,4,5,7]pentoxocane] with alpha,omega-diaminoalkanes in THF in the presence of Sm(NO3)(3)center dot 6 H2O as catalyst.
引用
收藏
页码：378 / 384
页数：7
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