Study on the effect of acid-heat coupling on the damage characteristics of coal pore-fissure structure

被引:13
|
作者
Xun Meng [1 ]
Xie Jingna [1 ]
Xie Jun [1 ]
Sun Qian [1 ]
Lu Shouqing [2 ]
Wang Gang [1 ]
机构
[1] Shandong Univ Sci & Technol, Minist Sci & Technol, State Key Lab Min Disaster Prevent & Control Cofo, Qingdao 266590, Peoples R China
[2] Qingdao Univ Technol, Dept Safety Engn, Qingdao 266520, Peoples R China
基金
中国国家自然科学基金; 中国博士后科学基金;
关键词
Acid-heat coupling; Pore structure; Microstructure; Energy dispersive spectrometry; Mercury intrusion porosimetry; ADSORPTION; NITROGEN;
D O I
10.1016/j.apt.2021.07.019
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
To study the effect of acid-heat coupled fracturing on the damage of coal pores and fractures, scanning electron microscope-energy dispersive spectrometry (SEM-EDS), mercury intrusion porosimetry (MIP) were used to analyze. The results of the study show that the acid-heat coupling effect not only changes the microscopic morphology and element composition of the coal sample, but also promotes the formation of a pore-fracture network within the coal, and the connectivity is significantly increased, which is conducive to the diffusion and migration of coalbed methane. The optimum acidification temperature for the experiment is 50 degrees C. SEM observed that the acid-heat coupling changed the local stress sensitivity of the coal body and weakens the strength of the coal body to form a fracture network. EDS analysis shows that the element distribution on the coal surface changes regularly with the increase of acidification temperature, and the reduction rate of mineral content on the coal surface is highest at 50 degrees C. MIP and fitting analysis show that the pore parameters of coal samples will increase with the increase of acid-heat coupling temperature, reaching a peak at 50 degrees C, and the acidification effect will be relatively slow after increasing the temperature. This research is of great significance for exploring the optimal acidification conditions of coal mines, reducing acidizing fracturing costs, and ensuring coal mine safety production. (c) 2021 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.
引用
收藏
页码:3425 / 3435
页数:11
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