Synthesis and Crystal Structure of 2-[(3-Bromo-phenylimino)methyl]phenol

被引：0
|
作者：
Guo, Ya-Ning [1 ]
机构：
[1] Baoji Univ Arts & Sci, Dept Chem & Chem Engn, Baoji, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2013年 / 25卷 / 07期
关键词：
Salicylaldehyde; Schiff base; Synthesis; Crystal structure; PI-PI STACKING; COMPLEXES; METAL;
D O I：
10.14233/ajchem.2013.13769
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new Schiff base 2-[(3-bromo-phenylimino)methyl]phenol, derived from condensation of salicylaldehyde with m-bromoaniline, has been prepared and characterized by single crystal X-raydiffraction. Schiff base is in the monoclinic system, space group (P21) with a = 3.928(14) angstrom, b = 10.590(4)angstrom, c = 13.212(5)angstrom, beta = 97.360(4)degrees, Mr = 276.13, V = 545.1(3)angstrom(3), D-e = 1.682 g/cm(3), Z = 2, mu = 3.745 mm-1, F-(000) = 276, R = 0.0326, wR = 0.0455. The schiff base is stabilized by intermolecular C-H center dot center dot center dot O and pi center dot center dot center dot pi interaction and further linked into a 2D layer structure.
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收藏
页码：3762 / 3764
页数：3
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