Preparation of nanometer-sized nickel oxide by hydrothermal decomposition

被引：2

作者：

Song, Yan ^{[1
]}

Wei, Chang ^{[1
]}

Li, Cunxiong ^{[1
]}

Xu, Hongsheng ^{[1
]}

Deng, Zhigan ^{[1
]}

Liu, Daqiang ^{[1
]}

机构：

[1] Kunming Univ Sci & Technol, Fac Met & Energy Engn, Kunming, Peoples R China

来源：

NEW MATERIALS, APPLICATIONS AND PROCESSES, PTS 1-3 | 2012年 / 399-401卷

关键词：

hydrothermal decomposition; precursor; nanometer-sized nickel oxide; ELECTROCHROMIC APPLICATIONS; BATTERIES; FILMS; NIO;

D O I：

10.4028/www.scientific.net/AMR.399-401.698

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

We prepared nanometer-sized nickel oxide by hydrothermal decomposition. In this work, NiSO4 center dot 6H(2)O and Na2CO3 were used as raw materials to prepare the precursors. Nanometer-sized nickel oxide was obtained after calcining the precursors. The temperature of the calcination process affects the morphology and size of the nanometer-sized nickel oxide. The precursors and products were analyzed by TG, XRD and SEM. Sheet nanometer-sized nickel oxide was obtained and characterized by its high purity, smooth surface, regular hexagon shape, average size of 500 nm and 30-60 nm thickness. The results indicate that the NiO particles become open pore structures at a calcination temperature above 500 degrees C.

引用

页码：698 / 703

页数：6

共 50 条

[31] A controllable nanometer-sized valve
Yu, Miao
Falconer, John L.
Amundsen, Ted J.
Hong, Mei
Noble, Richard D.
ADVANCED MATERIALS, 2007, 19 (19) : 3032 - +
[32] Chiral nanometer-sized structures
Nolte, RJM
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1996, 212 : 309 - ORGN
[33] Nanometer-sized molecular complexes
Papaefthymiou, GC
HYPERFINE INTERACTIONS, 1998, 113 (1-4): : 357 - 367
[34] ELECTROCHEMISTRY AT NANOMETER-SIZED ELECTRODES
PENNER, RM
HEBEN, MJ
LONGIN, TL
LEWIS, NS
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1991, 201 : 49 - ANYL
[35] Nanometer-sized electrochemical sensors
Shao, YH
Mirkin, MV
Fish, G
Kokotov, S
Palanker, D
Lewis, A
ANALYTICAL CHEMISTRY, 1997, 69 (08) : 1627 - 1634
[36] Elasticity of nanometer-sized objects
Segall, DE
Ismail-Beigi, S
Arias, TA
PHYSICAL REVIEW B, 2002, 65 (21)
[37] Hydrothermal preparation of nanometer lithium nickel vanadium oxide powder at low temperature
Lu, CH
Liou, SJ
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY, 2000, 75 (01): : 38 - 42
[38] Controlled hydrothermal synthesis, structural and optical analysis of nanometer-sized ZnO spheres
Pandey, Padmini
Kurchania, Rajnish
Hague, Fozia Z.
OPTIK, 2015, 126 (02): : 301 - 303
[39] Controlled preparation of nanometer-sized cylinder crystals of poly(ethylene oxide) embedded in methacrylate matrices.
Beginn, U
Fischer, E
Pieper, T
Mellinger, F
Kimmich, R
Möller, M
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1999, 218 : U408 - U408
[40] Preparation and gas sensitive properties of nanometer-sized SnO2
Pan, Qingyi
Dong, Xiaowen
Xu, Jiaqiang
Zhang, Jianping
Shi, Liyi
Journal of Shanghai University, 1998, 2 (01): : 72 - 76

← 1 2 3 4 5 →