A practical and efficient procedure for preparation of diacetals from 2,2-bis(hydroxymethyl)propane-1,3-diol with aldehydes and ketones catalysed by anhydrous ferrous sulfate

被引：10

作者：

Jin, TS ^{[1
]}

Ma, YR ^{[1
]}

Li, TS ^{[1
]}

Wang, JX ^{[1
]}

机构：

[1] Hebei Univ, Dept Chem, Baoding 071002, Peoples R China

来源：

JOURNAL OF CHEMICAL RESEARCH-S | 1999年 / 04期

关键词：

D O I：

10.1039/a900025i

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Synthesis of diacetals in excellent yields from aldehydes and ketones with 2,2-bis(hydroxymethyl) propane-1,3-diol is carried out in refluxing benzene or toluene with anhydrous ferrous sulfate as catalyst.

引用

页码：268 / 269

页数：2

共 28 条

[21] PHOSPHORUS-NITROGEN COMPOUNDS .65. THE REACTIONS OF HEXACHLOROCYCLOTRI-PHOSPHAZATRIENE WITH DIETHYL BIS-(HYDROXYMETHYL)MALONATE - COMPARISON OF PRODUCT TYPE AND OF THE P-31, H-1 AND C-13 NUCLEAR-MAGNETIC-RESONANCE SPECTRA WITH THE SPIRO DERIVATIVES OF PROPANE-1,3-DIOL AND 2,2-DIMETHYLPROPANE-1,3-DIOL
ALKUBAISI, AH
SHAW, RA
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1991, 55 (1-4): : 49 - 57
[22] New applications of solid silica chloride (SiO2-Cl) in organic synthesis.: Efficient preparation of diacetals of 2,2-bis(hydroxymethyl)-1,3-propanediol from different substrates and their transthioacetalization reactions.: Efficient regeneration of carbonyl compounds from acetals and acylals
Firouzabadi, H
Iranpoor, N
Hazarkhani, H
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2002, 177 (12) : 2847 - 2858
[23] Synthesis and stereochemistry of new 1,3-thiazolidine systems based on 2-amino-2-(mercaptomethyl)propane-1,3-diol: 4,4-bis(hydroxymethyl)-1,3-thiazolidines and c-5-hydroxymethyl-3-oxa-7-thia-r-1-azabicyclo[3.3.0]octanes
Morar, Cristina
Sacalis, Carmen
Lameiras, Pedro
Soran, Albert
Khartabil, Hassan
Antheaume, Cyril
Bratu, Ioan
Moldovan, Oana
Darabantu, Mircea
TETRAHEDRON, 2013, 69 (47) : 9966 - 9985
[24] An efficient and convenient method for preparation of 2,2-disubstituted and 2-monosubstituted 1,3-benzodioxoles from ketones and aldehydes with catechol catalysed by ZrO2/SO42-
Jin, TS
Zhang, SL
Wang, XF
Guo, JJ
Li, TS
JOURNAL OF CHEMICAL RESEARCH-S, 2001, (07): : 289 - 291
[25] Synthesis of 2,6,10,14,18,22-hexaazaspiro[11.11]tricosane, the first example of a spiro aza crown derived from 2,2-bis(aminomethyl)propane-1,3-diamine
Wang, Q
Mikkola, S
Lönnberg, H
TETRAHEDRON LETTERS, 2001, 42 (14) : 2735 - 2737
[26] An improved procedure for the preparation of 2,2-bis[2-[4(S)-tert-butyl-1,3-oxazolinyl]]propane [(S,S)-tert-butylbis(oxazoline)] and derived copper(II) complexes
Evans, DA
Peterson, GS
Johnson, JS
Barnes, DM
Campos, KR
Woerpel, KA
JOURNAL OF ORGANIC CHEMISTRY, 1998, 63 (13): : 4541 - 4544
[27] Improved procedure for the preparation of 2,2-bis[2-[4(S)-tert-butyl-1,3-oxazolinyl]]propane ((S,S)-tert-butylbis(oxazoline)) and derived copper(II) complexes
Evans, David A.
Peterson, Gretchen S.
Johnson, Jeffrey S.
Barnes, David M.
Campos, Kevin R.
Woerpel, Keith A.
Journal of Organic Chemistry, 1999, 64 (02):
[28] An improved procedure for the preparation of 2,2-bis[2-[4(S)-tert-butyl-1,3-oxazolinyl]]propane((S,S)-tert-butylbis(oxazoline)) and derived copper(II) complexes (vol 63, pg 4543, 1998)
Evans, DA
Peterson, GS
Johnson, JS
Barnes, DM
Campos, KR
Woerpel, KA
JOURNAL OF ORGANIC CHEMISTRY, 1999, 64 (02): : 678 - 678

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