A practical and efficient procedure for preparation of diacetals from 2,2-bis(hydroxymethyl)propane-1,3-diol with aldehydes and ketones catalysed by anhydrous ferrous sulfate

被引：10

作者：

Jin, TS ^{[1
]}

Ma, YR ^{[1
]}

Li, TS ^{[1
]}

Wang, JX ^{[1
]}

机构：

[1] Hebei Univ, Dept Chem, Baoding 071002, Peoples R China

来源：

JOURNAL OF CHEMICAL RESEARCH-S | 1999年 / 04期

关键词：

D O I：

10.1039/a900025i

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Synthesis of diacetals in excellent yields from aldehydes and ketones with 2,2-bis(hydroxymethyl) propane-1,3-diol is carried out in refluxing benzene or toluene with anhydrous ferrous sulfate as catalyst.

引用

页码：268 / 269

页数：2

共 28 条

[1] A Practical and Efficient Procedure for Preparation of Diacetals from 2,2-Bis(hydroxymethyl) propane-1,3-diol with Aldehydes and Ketones Catalysed by Anhydrous Ferrous Sulfate
厦门大学学报(自然科学版), 1999, (S1) : 285 - 285
[2] Montmorillonite clays catalysis. Part 12. An efficient and practical procedure for synthesis of diacetals from 2,2-bis(hydroxymethyl)propane-1,3-diol with carbonyl compounds
Zhang, ZH
Li, TS
Jin, TS
Li, JT
JOURNAL OF CHEMICAL RESEARCH, 1998, (10) : 640 - 641
[3] Potential Energetic Plasticizers on the Basis of 2,2-Dinitropropane-1,3-diol and 2,2-Bis(azidomethyl)propane-1,3-diol
Hafner, Sven
Hartdegen, Vera A.
Hofmayer, Maximilian S.
Klapoetke, Thomas M.
PROPELLANTS EXPLOSIVES PYROTECHNICS, 2016, 41 (05) : 806 - 813
[4] Polyurethanes based on 2,2-dinitropropane-1,3-diol and 2,2-bis(azidomethyl) propane-1,3-diol as potential energetic binders
Bellan, Andreas B.
Hafner, Sven
Hartdegen, Vera A.
Klapoetke, Thomas M.
JOURNAL OF APPLIED POLYMER SCIENCE, 2016, 133 (40)
[5] 2,2′-(p-Phenylenedimethylene)bis(propane-1,3-diol)
Gao, Yajun
Xi, Haitao
Sun, Xiaoqiang
Fu, Yongsheng
Liu, Li
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O170 - U2745
[6] An efficient procedure for the synthesis of diacetals from the InCl3•4H2O catalysed reaction of 2,2-bis (hydroxymethyl)-1,3-propanediol with aldehydes or ketones
Deng, GS
Ren, TG
JOURNAL OF CHEMICAL RESEARCH-S, 2003, (01): : 24 - 25
[7] 2,2-Bis(methoxy- and ethoxy-NNO-azoxy)propane-1,3-diol sulfonates
I. N. Zyuzin
Russian Journal of Organic Chemistry, 2014, 50 : 631 - 634
[8] 2,2-Bis(methoxy- and ethoxy-NNO-azoxy)propane-1,3-diol sulfonates
Zyuzin, I. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2014, 50 (05) : 631 - 634
[9] The mixed diol-dithiol 2,2-bis(sulfanylmethyl)propane-1,3-diol: characterization of key intermediates on a new synthetic pathway
Simmons, Trevor R.
Pickett, Christopher J.
Wright, Joseph A.
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2011, 67 : O1 - O5
[10] 2,2-Bis(hydroxymethyl)propane-1,3-diyl bis(1H-pyrrole-2-carboxylate)
Wang, JY
Yin, ZM
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O230 - O232

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