Structural analysis of PM biocomposites based on hydroxyapatite nanopowders elaborated by spark plasma sintering route

被引：0
|
作者：
Bebe-Adrian, Olei [1 ]
Oana, Gingu [1 ]
Nicoleta, Lupu [2 ]
Gabriela, Sima [1 ]
机构：
[1] Univ Craiova, Fac IMST, 1st Calugareni St, RO-220037 Dr Tr Severin, Mehedinti, Romania
[2] Natl Inst Chem Phys, RO-700050 Boulevard, Lasi, Romania
来源：
ADVANCED MATERIALS AND STRUCTURES IV | 2012年 / 188卷
关键词：
COATINGS;
D O I：
10.4028/www.scientific.net/SSP.188.52
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The objective of this research is the development of a detailed structural analysis of biocomposites with ceramic matrix of hydroxyapatite (Hap) reinforced by titanium (Ti), elaborated by powder metallurgy technology. Nanometric Hap powders (<200nm) 75% wt and micrometric Ti powders (<150 mu m) are homogenized in a high energy ball mill Pulverisette 6. Spark plasma sintering (SPS) is the sintering route able to lead to nanostructured sintered samples when nanopowders are used as raw material. The SPS parameters are: the sintering temperature, T=(1000-1100)degrees C and the maintaining time, t=(10-20) minutes in vacuum. The influence of the sintering parameters on the composites structures is monitored using the optical microscopy (OM), electronic microscopy (SEM) and the X-Ray diffraction (XRD).
引用
收藏
页码：52 / +
页数：2
相关论文
共 50 条
  • [31] Synthesis of Ti-based glassy alloy/hydroxyapatite composite by spark plasma sintering
    Zhu, Shengli
    Wang, Xinmin
    Yoshimura, Masahiro
    Inoue, Akihisa
    MATERIALS TRANSACTIONS, 2008, 49 (03) : 502 - 505
  • [32] Spark-Plasma-Sintering (SPS) of tungsten carbide and titanium carbonitride nanopowders
    Zalite, I.
    Angerer, P.
    Yu, L. G.
    Khor, K. A.
    ANNUAL CONFERENCE ON FUNCTIONAL MATERIALS AND NANOTECHNOLOGIES - FM&NT 2011, 2011, 23
  • [33] Spark plasma sintering of cobalt ferrite nanopowders prepared by coprecipitation and hydrothermal synthesis
    Millot, N.
    Le Gallet, S.
    Aymes, D.
    Bernard, F.
    Grin, Y.
    JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2007, 27 (2-3) : 921 - 926
  • [34] Spark plasma sintering of tungsten carbide nanopowders obtained through DC arc plasma synthesis
    Chuvil'deev, V. N.
    Blagoveshchenskiy, Yu. V.
    Nokhrin, A. V.
    Boldin, M. S.
    Sakharov, N. V.
    Isaeva, N. V.
    Shotin, S. V.
    Belkin, O. A.
    Popov, A. A.
    Smirnova, E. S.
    Lantsev, E. A.
    JOURNAL OF ALLOYS AND COMPOUNDS, 2017, 708 : 547 - 561
  • [35] Nano Pores Evolution in Hydroxyapatite Microsphere during Spark Plasma Sintering
    Lin, C.
    Xiao, C.
    Shen, Z.
    SCIENCE OF SINTERING, 2011, 43 (01) : 39 - 46
  • [36] Densification process of OH controlled hydroxyapatite ceramics by spark plasma sintering
    Kawagoe, D.
    Koga, Y.
    Ishida, E. H.
    Ioku, K.
    WATER DYNAMICS, 2006, 833 : 39 - +
  • [37] Osteoblast interactions with various hydroxyapatite based biomaterials consolidated using a spark plasma sintering technique
    Xu, J. L.
    Khor, Khiam Aik
    Lu, Y. W.
    Chen, W. N.
    Kumar, R.
    JOURNAL OF BIOMEDICAL MATERIALS RESEARCH PART B-APPLIED BIOMATERIALS, 2008, 84B (01) : 224 - 230
  • [38] Dehydroxylation of hydroxyapatite in dense bulk ceramics sintered by spark plasma sintering
    Liu, Yi
    Shen, Zhijian
    JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2012, 32 (11) : 2691 - 2696
  • [39] Fabrication of nanostructured hydroxyapatite via hydrothermal synthesis and spark plasma sintering
    Guo, XY
    Xiao, P
    Liu, J
    Shen, ZJ
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2005, 88 (04) : 1026 - 1029
  • [40] Influence of Spark Plasma Sintering and Baghdadite Powder on Mechanical Properties of Hydroxyapatite
    Khandan, A.
    Karamian, E.
    Mehdikhani-Nahrkhalaji, M.
    Mirmohammadi, H.
    Farzadi, A.
    Ozada, N.
    Heidarshenas, B.
    Zamani, K.
    5TH INTERNATIONAL BIENNIAL CONFERENCE ON ULTRAFINE GRAINED AND NANOSTRUCTURED MATERIALS, UFGNSM15, 2015, 11 : 183 - 189
12345