Synthesis of chalcogeno[3-(pyrid-2-yl)-1-azaallyl]germanium complexes

被引：27
|
作者：
Leung, WP [1 ]
Chong, KH [1 ]
Wu, YS [1 ]
So, CW [1 ]
Chan, HS [1 ]
Mak, TCW [1 ]
机构：
[1] Chinese Univ Hong Kong, Dept Chem, Shatin, Hong Kong, Peoples R China
来源：
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY | 2006年 / 04期
关键词：
chalcogens; germanium; N ligands;
D O I：
10.1002/ejic.200500717
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reaction of [Ge{C(C5H4N-2)C(Ph)N(SiMe3)(2)}{N(SiMe3)C(Ph)C(SiMe3)(C5H4N-2)}] (1) and [Ge{N(SiMe3)C(Ph)C(SiMe3)(C5H4N-2))Cl] (2) with stoichiometric amounts of elemental chalcogens in toluene affords [Ge(E){C(C5H4N-2)C(Ph)N(SiMe3)(2))(N(SiMe3)C(Ph)C(SiMe3)(C5H4N-2)}] [E = S (3), Se (4)] and [Ge(E)IN(SiMe3)C(Ph)C(SiMe3)(C5H4N-2)}Cl] [E = S (5), Se (6)], respectively. Compounds 3-6 were characterized by X-ray analysis. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006).
引用
收藏
页码：808 / 812
页数：5
相关论文
共 50 条
  • [1] Synthesis and antiproliferative activity of some 3-(pyrid-2-yl)-pyrazolines
    Ciupa, Alexander
    De Bank, Paul A.
    Mahon, Mary F.
    Wood, Pauline J.
    Caggiano, Lorenzo
    MEDCHEMCOMM, 2013, 4 (06) : 956 - 961
  • [2] FLUORENONE DERIVATIVES .9. 3-(PYRID-2-YL)-FLUORENONE, "2-METHYL-3-(PYRID-2-YL)-FLUORENONE, AND 2-(3-METHYL-PYRID-2-YL)FLUORENONE
    CHARDONNENS, L
    SUNDERPLASSMANN, P
    STAUNER, T
    HELVETICA CHIMICA ACTA, 1979, 62 (03) : 657 - 666
  • [3] Chelate complexes of the pyrid-2-yl analogue of tetracyclone
    Siemeling, Ulrich
    Klemann, Thorsten
    Bruhn, Clemens
    Neumueller, Bernhard
    Dehnicke, Kurt
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2008, 634 (05): : 895 - 900
  • [4] STEREOSELECTIVE OLEFIN INSERTION REACTIONS OF CHIRAL (EBI)ZR(ETA(2)-PYRID-2-YL)(+) AND (EBTHI)ZR(ETA(2)-PYRID-2-YL)(+) COMPLEXES
    RODEWALD, S
    JORDAN, RF
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (10) : 4491 - 4492
  • [5] Synthesis and Characterization of Tris(bidentate) Ruthenium Complexes of Di(pyrid-2-yl)(methyl)amine
    Wu, Si-Hai
    Shao, Jiang-Yang
    Dai, Xiaojuan
    Cui, Xiuling
    Su, Hongmei
    Zhong, Yu-Wu
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2017, (24) : 3064 - 3071
  • [6] Synthesis and coordination chemistry of 1,1,1-tris-(pyrid-2-yl)ethane
    Santoro, Amedeo
    Sambiagio, Carlo
    McGowan, Patrick C.
    Halcrow, Malcolm A.
    DALTON TRANSACTIONS, 2015, 44 (03) : 1060 - 1069
  • [7] NOVEL RUTHENIUM COMPLEXES CONTAINING TRIS(PYRID-2-YL)METHOXY-METHANE
    WITHAM, LM
    HUYNH, MHV
    SZCZEPURA, LF
    KRAJOWSKI, L
    CHURCHILL, MR
    TAKEUCHI, KJ
    JAMESON, DL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 210 : 462 - INOR
  • [8] NEW RUTHENIUM COMPLEXES CONTAINING TRIS(PYRID-2-YL)METHOXY-METHANE
    WITHAM, LM
    HUYNH, MHV
    SZCZEPURA, LF
    GONG, PK
    KRAJOWSKI, L
    CHURCHILL, MR
    TAKEUCHI, KJ
    JAMESON, DL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1995, 210 : 390 - INOR
  • [9] COMPLEXES OF 3-AMINO(PYRID-2-YL)THIOUREA WITH COPPER(II), COBALT(II) AND NICKEL(II)
    PATEL, RK
    PATEL, RN
    JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 1990, 67 (07) : 538 - 540
  • [10] (Spectro)Electrochemistry of 3-(Pyrid-2-yl)-s-Tetrazine- and 1,2-(Dihydro)pyridazine Tricarbonylrhenium(I)chloride
    Schnierle, Marc
    Winkler, Mario
    Filippou, Vasileios
    van Slageren, Joris
    Ringenberg, Mark R.
    EUROPEAN JOURNAL OF INORGANIC CHEMISTRY, 2022, 2022 (10)
12345