Hydrothermal Synthesis and Crystal Structure of a New Cd(II) Coordination Polymer With pcu Topological Net

被引：1

作者：

Zou, Guanglong ^{[1
]}

Wang, Xuelin ^{[2
]}

Du, Jie ^{[3
]}

Xie, Bing ^{[1
]}

机构：

[1] Guizhou Minzu Univ, Sch Chem & Environm Sci, Guiyang 550025, Peoples R China

[2] Guizhou Minzu Univ, Sch Sci, Guiyang 550025, Peoples R China

[3] Guiyang Univ, Coll Chem & Mat Engn, Guiyang, Peoples R China

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2016年 / 46卷 / 02期

关键词：

Cd(II); coordination polymer; crystal structure; METAL-ORGANIC FRAMEWORKS; PHOTOLUMINESCENT PROPERTIES; LIGAND; ACID; IMIDAZOLE;

D O I：

10.1080/15533174.2014.988242

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new Cd() coordination polymer with 1,4-phenylenediacetic acid (H(2)PDA) and 1,4-bis(3-pyridylmethy)piperazine (BPMP) has been prepared by hydrothermal synthesis and characterized by single-crystal X-ray diffraction and IR. Complex{[Cd(PDA) (BPMP)] 4 (H2O)}(n) (1) is triclinic, space group P-1 with a = 10.443 (5), b = 11.542 (5), c = 13.197 (5) angstrom, = 87.510 (5)degrees, = 70.648 (5)degrees, = 85.711 (5)degrees, V = 1496.3 (11) angstrom(3), Z = 2, M-r = 648.99, D-c = 1.432g/cm(3), F(000) = 664, and mu = 0.781mm(-1). The final refinement gave R = 0.0571 and wR = 0.0616 for 6184 reflections with I > 2 sigma(I). X-ray diffraction analysis reveals that the complex 1 displays three-dimensional structure with a pcu topological net.

引用

页码：295 / 298

页数：4

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