X-ray microscopy of multiphase polymeric materials

被引：3
|
作者：
Ade, H
Smith, AP
Zhuang, GR
Wood, B
Plotzker, I
Rightor, E
Liu, DJ
Lui, SC
Sloop, C
机构：
来源：
APPLICATIONS OF SYNCHROTRON RADIATION TECHNIQUES TO MATERIALS SCIENCE III | 1996年 / 437卷
关键词：
D O I：
10.1557/PROC-437-99
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
We have utilized the scanning transmission x-ray microscope at Brookhaven National Laboratory to acquire high energy resolution spectra of various polymers and to investigate the bulk characteristics of multiphasic polymeric materials with chemical sensitivity at a spatial resolution of about 50 nm. We present studies ranging from phase separated liquid crystalline polyesters and polyurethanes to various polymer blends. Improvements in the NEXAFS imaging and spectral acquisition protocol in the recent past provide much improved spectral fidelity and include in situ energy calibration with CO2.
引用
收藏
页码：99 / 105
页数：7
相关论文
共 50 条
  • [1] The Combination of Electron Microscopy, Raman Microscopy and Energy Dispersive X-Ray Spectroscopy for the Investigation of Polymeric Materials
    Schmidt, Ruth
    Fitzek, Harald
    Nachtnebel, Manfred
    Mayrhofer, Claudia
    Schroettner, Hartmuth
    Zankel, Armin
    MACROMOLECULAR SYMPOSIA, 2019, 384 (01)
  • [2] X-ray crystallographic studies of polymeric materials
    Bhat, NV
    Deshmukh, RR
    INDIAN JOURNAL OF PURE & APPLIED PHYSICS, 2002, 40 (05) : 361 - 366
  • [3] System of x-ray identification of substantially multiphase materials
    I. S. Yakimov
    Inorganic Materials, 2008, 44 : 1531 - 1535
  • [4] System of x-ray identification of substantially multiphase materials
    Yakimov, I. S.
    INORGANIC MATERIALS, 2008, 44 (14) : 1531 - 1535
  • [5] THE APPLICATION OF X-RAY MICROSCOPY IN MATERIALS SCIENCE
    CUNNINGHAM, TG
    DAVIES, RL
    GRAHAM, SC
    JOURNAL OF MICROSCOPY-OXFORD, 1986, 144 : 261 - 275
  • [6] X-ray and electron microscopy of actinide materials
    Moore, Kevin T.
    MICRON, 2010, 41 (04) : 336 - 358
  • [7] Compositional and orientational characterization of polymeric systems with X-ray microscopy
    Ade, H
    TRENDS IN POLYMER SCIENCE, 1997, 5 (02) : 58 - 66
  • [8] Focused issue on X-ray microscopy of biological materials
    Carrascosa, Jose L.
    Glaeser, Robert M.
    JOURNAL OF STRUCTURAL BIOLOGY, 2012, 177 (02) : 177 - 178
  • [9] X-RAY MICROSCOPY AND X-RAY MICROANALYSIS
    COSSLETT, VE
    NATURE, 1959, 184 (4690) : 860 - 862
  • [10] RECENT DEVELOPMENTS IN X-RAY PROJECTION MICROSCOPY AND X-RAY MICROTOMOGRAPHY APPLIED TO MATERIALS SCIENCE
    CAZAUX, J
    ERRE, D
    MOUZE, D
    PATAT, JM
    RONDOT, S
    SASOV, A
    TREBBIA, P
    ZOLFAGHARI, A
    JOURNAL DE PHYSIQUE IV, 1993, 3 (C7): : 2099 - 2104
12345