Two New Compounds from the Roots of Ilex pubescens

被引:1
|
作者
Chen, Jing [1 ,2 ]
Liang, Hong [1 ,2 ]
Wu, Yuling [1 ,2 ]
Ji, Hongyan [1 ,2 ]
Liu, Cheng [1 ,2 ,3 ]
Fu, Xueyan [1 ,2 ]
Zhang, Xinhui [1 ,2 ]
Wang, Jianhuan [1 ,2 ]
Lin, Dong [1 ,2 ]
Gao, Xiaojuan [1 ,2 ]
Quan, Hongfeng [1 ,2 ]
Zhao, Yunsheng [1 ,2 ]
Wang, Jinhui [4 ]
Wu, Xiuli [1 ,2 ]
机构
[1] Ningxia Med Univ, Sch Pharm, Ningxia 750004, Peoples R China
[2] Ningxia Res Ctr Modern Hui Med Engn & Technol, Ningxia 750004, Peoples R China
[3] Ningxia Med Univ, Med Sci Ctr, Ningxia 750004, Peoples R China
[4] Shengyang Pharmaceut Univ, Sch Tradit Chinese Med, Shenyang 110016, Liaoning, Peoples R China
关键词
Ilex pubescens; ilexin L-1; ilexin L-3; roots; TRITERPENE;
D O I
10.1007/s10600-013-0762-2
中图分类号
R914 [药物化学];
学科分类号
100701 ;
摘要
Two new compounds, named ilexin L-1 and ilexin L-3, were isolated from the roots of Ilex pubescens. Their structures were elucidated as 1-[3-formyl-2-methoxyacetyl-(E)-3-pentenyl] cycloolivil ketal (1) and rhodioside-4,6-O-2'-methoxylacetyl-3'-formyl-(E)-3-pentenyl-beta-D-glucoside (2), respectively. The absolute configuration in compound 1 was assigned as 7'S, p8'S, 8S,10R on the basis of the CD spectrum, and compound 2 was assigned as 7R on the basis of the NOESY spectrum and chemical methods.
引用
收藏
页码:848 / 851
页数:4
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