1-N,2-O-carbonyl-3,5-O-isopropylidene-1-N-[(2R)-2-methyl-3-oxopentanoyl]-α-D-xylofuranosylamine

被引：0
|
作者：
Kopf, J
Lützen, A
Köll, P
机构：
[1] Univ Hamburg, Inst Anorgan & Angew Chem, D-20146 Hamburg, Germany
[2] Univ Oldenburg, Fachbereich Chem, D-26111 Oldenburg, Germany
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1999年 / 55卷
关键词：
D O I：
10.1107/S0108270199007210
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The title compound, C15H21NO7, was synthesized as part of a study involving the testing of new carbohydrate-derived chiral auxiliaries. Its solid-state conformation and absolute configuration were determined. The R configuration for the chiral centre at C-22, created during the synthesis, was deduced from knowledge of the absolute structure of the D-xylose moiety.
引用
收藏
页码：1541 / 1542
页数：2
相关论文
共 50 条
  • [1] 3,5-O-isopropylidene-2-C-methyl-D-xylonolactone
    Watkin, DJ
    Parry, LL
    Hotchkiss, DJ
    Eastwick-Field, V
    Fleet, GWJ
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3302 - O3303
  • [2] Tetrakis(6-methyl-2,2′-bipyridine)-1κ2N,N′;2κ2N,N′;3κ2N,N′;4κ2N,N′-tetra-μ-nitrato-1:2κ2O:O′;2:3κ3O:O′,O";2:3κ3O,O′:O";3:4κ2O:O′-tetranitrato-1κ4O,O′;4κ2O,O′-tetralead(II)
    Ahmadi, Roya
    Kalateh, Khadijeh
    Alizadeh, Robabeh
    Khoshtarkib, Zeinab
    Amani, Vahid
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : M1169 - +
  • [3] Resolution of 1-n-Butyl-3-Methyl-3-Phospholene 1-Oxide With TADDOL Derivatives and Calcium Salts of O, O'-Dibenzoyl-(2R,3R)- or O, O'-di-p-Toluoyl-(2R,3R)- tartaric Acid
    Bagi, Peter
    Fekete, Andras
    Kallay, Mihaly
    Hessz, Dora
    Kubinyi, Miklos
    Holczbauer, Tamas
    Czugler, Matyas
    Fogassy, Elemer
    Keglevich, Gyoergy
    CHIRALITY, 2014, 26 (03) : 174 - 182
  • [4] (-)-(2R, 3R)-O, O′-dibenzoyl-(2R, 3R)-tartaric acid-hexamethylphosphoramide (1/2)
    Zhang, Yi-Jian
    Shu, Zhan
    Feng, Wen-Jie
    Li, Mei-Chao
    Jin, Zhi-Min
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O1546 - O1548
  • [5] Bis(dimethylformamide-2κO)bis[μ-1(2-oxidobenzoyl)-2-(phenoxyacetyl)hydrazine(3-)]-1κ3O,N,O′: 2κ2N,O"-2κ2N,O":3κ3O,N,O′-dipyridine-1κN,3κN-trinickel(II)
    Zhao, Yan
    Luo, Jian-Hai
    Huang, Xi-He
    Huang, Chang-Cang
    Liu, Dong-Sheng
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : M1999 - U1901
  • [6] Bis(μ-3,5-dinitrobenzoato-κ2O1:O1′)bis(μ-3,5-dinitrobenzoato)-κ3O1,O1′:O1;κ3O1:O1,O1′-bis[(3,5-dinitrobenzoato-κ2O1,O1′)(1,10-phenanthroline-κ2N,N)dysprosium(III)]
    Dong, Chun-Hua
    Zhang, Da-Hai
    Ren, Ning
    Xi, Gai-Qing
    Hao, Juan-Juan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : M102 - U1070
  • [7] A practical synthesis of (2R)-3,5-di-O-benzoyl-2-fluoro-2-C-methyl-D-ribono-γ-lactone
    Zhang, Pingsheng
    Iding, Hans
    Cedilote, Miall
    Brunner, Stephan
    Williamson, Thomas
    Cleary, Thomas P.
    TETRAHEDRON-ASYMMETRY, 2009, 20 (03) : 305 - 312
  • [8] Diaqua[(1R,2R)-N,N′-bis(3,5-dibromosalicylidene)cyclohexane-1,2-diamine-κ4O,N,N′,O′]manganese(III) perchlorate dihydrate
    Akitsu, T
    Takeuchi, Y
    Einaga, Y
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : M772 - M774
  • [9] μ-oxalato-κ2O1,O2:κ2O1′,O2′-bis[(3,5-dicarboxybenzoato-κ2O1,O1′)(1,10-phenanthroline-κ2N,N′)copper(II)]
    Qin, Chao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M1006 - M1007
  • [10] Bis[μ2-N,N′-bis(2-oxidobenzyl)propane-1,3-diamine]-1κ4O,N,N′,O′:2κ2O,O′:2κ2O,O′:3κ4O,N,N′,O′-bis(N,N′-dimethylformamide)1κO,3κO-di-μ2acetato-1:2κ2O: O′;2:3κ2O:;O′dinickel(II)zinc(II)
    Yildirim, Leyla Tatar
    Ergun, Uemit
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : m2424 - m2425
12345