Synthesis of acyl[35S]sulfonamides: Coupling of high specific activity [35S]methane sulfonamide with acids and acid chlorides

被引：0

作者：

Wallace, Michael ^{[1
]}

Allentoff, Alban J. ^{[1
]}

Bonacorsi, Samuel, Jr. ^{[1
]}

机构：

[1] Bristol Myers Squibb Co, Radiochem, Princeton, NJ 08543 USA

来源：

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS | 2012年 / 55卷 / 13期

关键词：

35S]methanesulfonamide; 35S]methanesulfonyl chloride; acyl sulfonamide; ARYL;

D O I：

10.1002/jlcr.2974

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Direct coupling of high specific activity [35S]methanesulfonamide, generated from [35S]methanesulfonyl chloride and ammonia, with acids and acid chlorides afforded the corresponding [35S]acyl sulfonamides in excellent yields. Examples of high specific activity [35S]acyl sulfonamides were prepared containing functionality that can be further elaborated through carboncarbon or carbonnitrogen bond forming reactions.

引用

页码：474 / 476

页数：3

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