Comparison of some different extraction techniques for some organic pollutants in contaminated soils

被引:0
|
作者
Zuloaga, O [1 ]
Etxebarria, N [1 ]
Fernández, LA [1 ]
Madariaga, JM [1 ]
机构
[1] Euskal Herriko Unibertsitatea, Kimika Analitikoaren Saila, E-48080 Bilbao, Spain
来源
QUIMICA ANALITICA | 2001年 / 20卷 / 03期
关键词
microwave-assisted extraction; accelerated solvent extraction; soxhlet extraction; phenols; PCBs; PAHs; DDT; HCH isomers; soil analysis;
D O I
暂无
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Previously optimised closed microwave-assisted extraction, focused microwave-assisted extraction and accelerated solvent extraction methods were studied for the extraction of a variety of organic pollutants (phenols, PCBs, HCH isomers, DDT its metabolites and PAHs) from soil samples. In most cases, the results obtained were compared with,traditional Soxhlet extraction and reference materials (CRM, 481 and CRM 524) were used. In all cases, the recoveries and repeatabilities ties obtained with the developed new methods were better or at least comparable with the results obtained with Soxhlet extraction and the results were in good agreement with referenced values.
引用
收藏
页码:131 / 137
页数:7
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