1H, 13C, 19Sn NMR, mass, Mossbauer and biological studies of tri-, di- and chlorodiorganotin(IV) carboxylates

被引：0
|
作者：
Masood, H
Ali, S [1 ]
Mazhar, M
Shahzadi, S
Shahid, K
机构：
[1] Quaid I Azam Univ, Dept Chem, Islamabad 45320, Pakistan
[2] Natl Phys & Standards Lab, Islamabad, Pakistan
来源：
TURKISH JOURNAL OF CHEMISTRY | 2004年 / 28卷 / 01期
关键词：
D O I：
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中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The reaction of 2-[(2,3-dimethylphenyl)aminol]benzoic acid (HL) with tri- and diorganotin (IV) chlorides yielded complexes of the type R3SnL and R2SnL2 (R = n-C4H9, C6H5, C6H5CH2, n-C8H17). The compounds R2SnCIL were obtained by a redistribution reaction between R2SnL2 and R2SnCl2. All the compounds were characterized by CHN analysis, infrared, multinuclear NMR, mass and Mossbauer spectroscopy. The possible mode of carboxylate group bonding in solid as well as in solution is proposed on the basis of infrared, Mossbauer and NMR (H-1, C-13: (119)Su) spectroscopy.
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页码：75 / 85
页数：11
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