Crystal structure and Hirshfeld surface analysis of (E)-2-[1-hydroxy-2-(pyridin-2-yl)ethyl]-4-[2-(4-methoxyphenyl)diazen-1-yl]phenol

被引：0
|
作者：
Faizi, Md Serajul Haque [1 ]
Sen, Pratik [2 ]
Saxena, Gyanesh Kumar [2 ]
Golenya, Irina A. [3 ]
机构：
[1] BRA Bihar Univ, Langat Singh Coll, Dept Chem, Muzaffarpur 842001, Bihar, India
[2] Indian Inst Technol Kanpur, Dept Chem, Kanpur 208016, Uttar Pradesh, India
[3] Natl Taras Shevchenko Univ, Dept Chem, Volodymyrska Str 64, UA-01601 Kiev, Ukraine
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2019年 / 75卷
关键词：
crystal structure; azo compounds; diazenyl; pyridine; hydrogen bonding; C-H center dot center dot center dot pi interactions; offset pi-pi interactions; supramolecular framework; Hirshfeld surface analysis;
D O I：
10.1107/S2056989019004377
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C20H19N3O3, the configuration about the azo N=N bond is E, and the central benzene ring is inclined to the pyridine ring by 31.43 (8)degrees and to the 4-methoxyphenyl ring by 4.73 (8)degrees. In the crystal, molecules are linked by pairs of O-H center dot center dot center dot N hydrogen bonds, forming inversion dimers with an R-2(2)(12) ring motif. The dimers are linked by O-H center dot center dot center dot O and C-H center dot center dot center dot O hydrogen bonds, forming layers parallel to the ac plane. There are C-H center dot center dot center dot pi interactions present within the layers and between the layers, leading to the formation of a supramolecular framework. The layers are alsolinked by offset pi-pi interactions, A with an interplanar distance of 3.416 (2) angstrom.
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页码：600 / +
页数：9
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