Preparation of Lead Sulfide/Silica Core-Shell Structure Submicron Particles by Ultrasonic Method

被引：0
|
作者：
Geng Qing-Fen [1 ,2 ]
Wang Xiao-Peng [1 ,2 ]
Zhang Xia [2 ,3 ]
Liu Gang [1 ]
机构：
[1] Chinese Acad Sci, Lanzhou Inst Chem Phys, Ctr Ecomat & Ecochem, Lanzhou 730000, Peoples R China
[2] Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
[3] Chinese Acad Sci, Lanzhou Inst Chem Phys, State Key Lab Solid Lubricat, Lanzhou 730000, Peoples R China
来源：
CHINESE JOURNAL OF INORGANIC CHEMISTRY | 2009年 / 25卷 / 08期
关键词：
lead sulfide nano-particles; ultrasonic; silica-coated; core-shell structure; SONOCHEMICAL SYNTHESIS; PBS; NANOCRYSTALS; NANOCUBES; EVOLUTION; NANORODS; ELECTRON; XPS;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
One kind of well-defined lead sulfide nano-particles was synthesized according to the literature method and characterized by FE-SEM and XRD. Then, silica-coated lead sulfide submicron particles were prepared with the aid of sonication in a short time. TEM, XRD and XPS were used to observe and analyze the shape and structure of the as-prepared lead sulfide/silica core-shell submicron particles. The results indicate that the lead sulfide nano-crystallines are well coated by amorphous silica with adjustable thickness. After preparation of lead sulfide/silica composite particles, their fluorescence property was further studied.
引用
收藏
页码：1497 / 1503
页数：7
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