Synthesis, spectroscopic characterization, and in vitro antioxidant activity of polyglycidylmethacrylate/polyindole conducting polymer composites

被引:2
|
作者
Alayunt, Naci Omer [1 ]
Soykan, Cengiz [2 ]
机构
[1] Univ Siirt, Med Fac, Siirt, Turkey
[2] Univ Usak, Dept Mat Sci & Nanotechnol Engn, Usak, Turkey
关键词
AFM; FT-IR; in vitro antioxidant activity; PGMA; PIN conducting polymer composite; SEM; TGA; ELECTROCHEMICAL PROPERTIES; MONOMER REACTIVITY; REDOX BEHAVIOR; POLYINDOLE; POLY(5-CYANOINDOLE); LICLO4-ACETONITRILE; FILMS; RAMAN; OIL;
D O I
10.1002/jemt.23591
中图分类号
R602 [外科病理学、解剖学]; R32 [人体形态学];
学科分类号
100101 ;
摘要
Polyglycidylmethacrylate/polyindole (PGMA/PIN) conducting polymer composites having five different compositions were prepared chemically using FeCl(3)as an oxidant agent in chloroform solution and nitrogen atmosphere at 10 degrees C. The conducting polymer composites were characterized by FTIR spectroscopic technique, scanning electron microscopy (SEM), atomic force microscopy (AFM), and thermogravimetric analysis (TGA) measurements. It is seen that morphological structure of composite is different from PIN and PGMA. PGMA/PIN conducting polymer composite including 50% of PIN has a nonuniform and less homogenous structure compared to the PIN and PGMA polymer. in vitro antioxidant activity such as reduction force, superoxide radical removal activity, hydroxyl radical trapping activity, MDA measurements inSaccharomyces cerevisiaecells of PGMA/PIN conducting polymer composite was investigated. It was observed that the reduction force capacities decreased as PIN content and increased due to the percentage of composite of PGMA content. in vitro studies of synthesized composites have shown us that these compounds possess new antioxidant properties.
引用
收藏
页码:326 / 336
页数:11
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