[1] Univ Nova Lisboa, UNIDEMI, Dept Mech & Ind Engn, NOVA Sch Sci & Technol, P-2829516 Caparica, Portugal
[2] Sao Paulo State Univ UNESP, Campus Sao Joao da Boa Vista, BR-13876750 Sao Joao Da Boa Vista, SP, Brazil
[3] Univ Sao Paulo, Met & Mat Engn Dept, Ave Prof Mello Moraes 2463, BR-05508030 Sao Paulo, SP, Brazil
[4] Univ Autonoma Barcelona, Serv Microscopia, E-08193 Bellaterra, Spain
[5] Helmholtz Zentrum Geesthacht, Inst Mat Res, Max Planck Str 1, D-21502 Geesthacht, Germany
[6] Univ Nova Lisboa, Dept Mat Sci, NOVA Sch Sci & Technol, CENIMAT I3N, P-2829516 Caparica, Portugal