Effect of vibro-milling time on phase formation and particle size of lead titanate nanopowders

被引：39

作者：

Wongmaneerung, R ^{[1
]}

Yimnirun, R ^{[1
]}

Ananta, S ^{[1
]}

机构：

[1] Chiang Mai Univ, Fac Sci, Dept Phys, Chiang Mai 50200, Thailand

来源：

MATERIALS LETTERS | 2006年 / 60卷 / 12期

关键词：

lead titanate; milling; nanopowders; phase formation; particle size;

D O I：

10.1016/j.matlet.2005.11.043

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

A perovskite-like phase of lead titanate, PbTiO3, nanopowder was synthesized by a solid-state reaction via a rapid vibro-milling technique. The effect of milling time on the phase formation and particle size of PbTiO3 powder was investigated. Powder samples were characterized using TG-DTA, XRD, SEM and laser diffraction techniques. It was found that an average particle size of 17 nm was achieved at 25 h of vibro-milling after which a higher degree of particle agglomeration was observed on continuation of milling to 35 h. In addition, by employing an appropriate choice of the milling time, a narrow particle size distribution curve was also observed. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：1447 / 1452

页数：6

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