Synthesis and Molecular Structure of 2-(4-Chlorophenyl)-3-(phenyl-amino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one

被引：0
|
作者：
Sharma, Devinder K. [1 ]
Subbulakshmi, K. N. [2 ]
Narayana, B. [2 ]
Sarojini, B. K. [3 ]
Anthal, Sumati [1 ]
Kant, R. [1 ]
机构：
[1] Univ Jammu, Dept Phys, Xray Crystallog Lab, Jammu, India
[2] Mangalore Univ, Dept Chem, Mangalagangothri, DK, India
[3] Mangalore Univ, Dept Ind Chem, Mangalagangothri, DK, India
来源：
CRYSTALLOGRAPHY REPORTS | 2017年 / 62卷 / 07期
关键词：
IMIDAZOLE; INHIBITION; RESINS;
D O I：
10.1134/S1063774517070082
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one, C20H14N3OSCl was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The crystals are triclinic, sp. gr. P1, Z = 2. All three rings are planar, and imidazole ring is almost perpendicular to the phenyl ring with the dihedral angle of 88.65(2)degrees. In the crystal, pairs of O-H center dot center dot center dot O hydrogen bonds link molecules into inversion dimers, featuring R-22(10) graph set motif. Crystal structure is further stabilized by pi center dot center dot center dot pi interactions.
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收藏
页码：1148 / 1151
页数：4
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