MICROWAVE-ASSISTED SOLVOTHERMAL SYNTHESIS OF POROUS ZINC OXIDE NANOSTRUCTURES

被引：0
|
作者：
de la Garza, Maria [1 ]
Lopez, Israel [1 ]
Avina, Felix [1 ]
Gomez, Idalia [1 ]
机构：
[1] UANL, Fac Ciencias Quim, Lab Mat 1, San Nicolos De Los Garza, Nuevo Leon, Mexico
来源：
JOURNAL OF OVONIC RESEARCH | 2013年 / 9卷 / 04期
关键词：
Zinc oxide; Microwave-assisted synthesis; Porous structure; ZNO; NANOPARTICLES; PHOTOLUMINESCENCE; ELECTRODEPOSITION; IRRADIATION; DIODES; ARRAYS;
D O I：
暂无
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Porous ZnO nanostructures were synthesized by reaction of zinc acetate dihydrate with water in 2-propanol solution via a facile microwave-assisted solvothermal method. The synthesis was carried out in a conventional microwave oven, using a closed container as solvothermal reactor. Controlled parameters were water concentration and microwave irradiation time. The obtained products were characterized by means of X-ray powder diffraction (XRD), UV-Vis spectrophotometry, Fourier transform infrared spectroscopy (FT-IR) and field emission scanning electron microscopy (FE-SEM). These nanoparticles have a minimum average diameter of 37 nm, which are agglomerated into irregular and spheroidal nanostructures with dimensions larger than 1 mu m and high porosity. Mesopores and macropores with hexagonal geometry were found in the nanostructures.
引用
收藏
页码：89 / 94
页数：6
相关论文
共 50 条
  • [21] Synthesis of Copper Oxide Nanostructures with Controllable Morphology by Microwave-Assisted Method
    Yan, Shancheng
    Shen, Kai
    Zhang, Yong
    Zhang, Yuping
    Xiao, Zhongdang
    [J]. JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2009, 9 (08) : 4886 - 4891
  • [22] Synthesis of potassium niobates by the microwave-assisted solvothermal method
    Duarte, T. M.
    Honorio, L. M. C.
    Brito, A. S.
    Souza, J. K. D.
    Longo, E.
    Tranquilin, R. L.
    Souza, A. G.
    Santos, I. M. G.
    Maia, A. S.
    [J]. BRAZIL MRS MEETING 2014, 2015, 97
  • [23] Microwave-assisted solvothermal synthesis of radial ZnS nanoribbons
    Liu, XY
    Tian, BZ
    Yu, CZ
    Tu, B
    Zhao, DY
    [J]. CHEMISTRY LETTERS, 2004, 33 (05) : 522 - 523
  • [24] Self-assembled zinc oxide nanostructures via a rapid microwave-assisted route
    Mohajerani, Matin Sadat
    Mazloumi, Mahyar
    Lak, Aidin
    Kajbafvala, Amir
    Zanganeh, Saeid
    Sadrnezhaad, S. K.
    [J]. JOURNAL OF CRYSTAL GROWTH, 2008, 310 (15) : 3621 - 3625
  • [25] Microwave-assisted synthesis of hierarchical ZnO nanostructures
    Tong, Laga
    Liu, Ye
    Rong, Hua
    Gong, Liangfa
    [J]. MATERIALS LETTERS, 2013, 112 : 5 - 7
  • [26] Microwave-Assisted Green Synthesis of Silver Nanostructures
    Nadagouda, Mallikarjuna N.
    Speth, Thomas F.
    Varma, Rajender S.
    [J]. ACCOUNTS OF CHEMICAL RESEARCH, 2011, 44 (07) : 469 - 478
  • [27] Microwave-assisted synthesis of metallic nanostructures in solution
    Tsuji, M
    Hashimoto, M
    Nishizawa, Y
    Kubokawa, M
    Tsuji, T
    [J]. CHEMISTRY-A EUROPEAN JOURNAL, 2005, 11 (02) : 440 - 452
  • [28] Microwave-assisted solvothermal synthesis of zirconium oxide based metal-organic frameworks
    Liang, Weibin
    D'Alessandro, Deanna M.
    [J]. CHEMICAL COMMUNICATIONS, 2013, 49 (35) : 3706 - 3708
  • [29] Microwave-assisted synthesis of zinc oxide and its performance in photodegradation of CTMAB
    Yanxiu Liu
    Hua Song
    Kenan Zhu
    Feng Li
    [J]. Research on Chemical Intermediates, 2017, 43 : 971 - 982
  • [30] Microwave-assisted synthesis of zinc oxide and its performance in photodegradation of CTMAB
    Liu, Yanxiu
    Song, Hua
    Zhu, Kenan
    Li, Feng
    [J]. RESEARCH ON CHEMICAL INTERMEDIATES, 2017, 43 (02) : 971 - 982
12345