Syntheses, Crystal Structures and Properties of Three Transition Metal Coordination Compounds Based on 2,2′-Bipyridine-3,3′,6,6′-tetracarboxylic Acid

被引：2
|
作者：
Bing Ying-Ying [1 ]
Wu Zhen-Ting [1 ]
Hu Ming [1 ]
机构：
[1] Inner Mongolia Univ, Sch Chem & Chem Engn, Inner Mongolia Key Lab Chem & Phys Rare Earth Mat, Hohhot 010021, Peoples R China
来源：
CHINESE JOURNAL OF INORGANIC CHEMISTRY | 2015年 / 31卷 / 10期
关键词：
2,2 '-bipyridine-3,3 ',6,6 '-tetracarboxylic acid; coordination compound; synthesis; crystal structure; COMPLEXES; POLYMERS;
D O I：
10.11862/CJIC.2015.264
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Three transition metal complexes, namely, [Co-2(H(2)bptc)(2)(H2O)(4)]center dot bpe center dot 9H(2)O (1), [Ni-2(H(2)bptc)(2)(H2O)(4)]center dot bpe center dot 9H(2)O (2), [Ni-2(H(2)bptc)(2)(H2O)(4)]center dot 0.5bpp center dot 7H(2)O (3) (H(4)bptc=2,2'-bipyridine-3,3',6,6'-tetracarboxylic acid, bpe=1,2-di(4-pyridyl)ethylene, bpp=1,2-di(4-pyridyl) ethane) have been synthesized under hydrothermal conditions and structurally characterized by infrared spectra, thermogravimetric analyses and single crystal X-ray diffraction. Compounds 1 similar to 3 are the mononuclear units and extended further to generate the three-dimensional supramolecular architectures by strong hydrogen-bonding interactions, respectively. CCDC: 1054309, 1; 1054310, 2; 1054311, 3.
引用
收藏
页码：2059 / 2064
页数：6
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