Four 3d-4d heterometallic coordination polymers based on 1,2,3-triazole-4,5-dicarboxylate: Synthesis, structures, and magnetic properties

被引：14
|
作者：
Sun, Ya-Guang [1 ]
Gao, Xin [1 ]
Xiong, Gang [1 ]
Zong, Wen-Hui [1 ]
Ding, Fu [1 ]
Xu, Zhen-He [1 ]
Wang, Shu-Ju [1 ]
You, Li-Xin [1 ]
Ren, Bao-Yi [1 ]
Gao, En-Jun [1 ]
机构：
[1] Shenyang Univ Chem Technol, Lab Coordinat Chem, Shenyang 100142, Peoples R China
来源：
INORGANICA CHIMICA ACTA | 2014年 / 409卷
关键词：
Heterometallic coordination polymers; Crystal structure; Magnetism; CRYSTAL-STRUCTURE; BUILDING-BLOCKS; MIXED-VALENCE; 3D; METAL; FRAMEWORKS; LUMINESCENT; 2D; LN; COMPLEXES;
D O I：
10.1016/j.ica.2013.09.039
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Four 3d-4d heterometallic coordination polymers, [Ag2M(HTzDC)(2)center dot 3H(2)O](n)(M = Co(1), Ni(2), Zn(3) and {[(CH3)(2)NH2][AgCu5(TzDC)(4)center dot 6H(2)O]center dot 6H(2)O]}(n)(4) (H(3)TzDC = 1,2,3-triazole-4,5-dicarboxylic acid) were synthesized under hydrothermal conditions using one-step approach and structurally characterized by elemental analysis, FT-IR, power X-ray diffraction and single-crystal X-ray diffraction. The single-crystal X-ray diffraction analysis reveals that complexes 1-3 are isostructural, the three dimensional frameworks is composed of Ag ions and transition metals which linked by TzDC ligands; the complex 4 exhibits a three-dimensional architecture constructed by planar {AgCu4N12} units. The magnetic properties of compounds 1-2 and 4 were investigated. (C) 2013 Elsevier B.V. All rights reserved.
引用
收藏
页码：497 / 502
页数：6
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