Determination of dymron in agricultural products by HPLC

被引：0
|
作者：
Kobayashi, M [1 ]
Nagayama, T [1 ]
Hashimoto, T [1 ]
Haneishi, N [1 ]
Ito, M [1 ]
Tamura, Y [1 ]
Takada, C [1 ]
Yasuda, K [1 ]
机构：
[1] Tokyo Metropolitan Res Lab Publ Hlth, Shinjuku Ku, Tokyo 1690073, Japan
来源：
JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN | 1999年 / 40卷 / 03期
关键词：
dymron; daimuron; agricultural products; HPLC; herbicide; UV detector; GC MS; LC MS;
D O I：
暂无
中图分类号：
TS2 [食品工业];
学科分类号：
0832 ;
摘要：
We investigated a simplified determination of dymron in agricultural products by HPLC with UV detection. Homogenates of agricultural products were extracted with acetone. Each crude extract was purified on Bond Elut(R) extraction Cartridge PSA and SAX using a mixture of acetonitrile and diethyl ether. Dymron was analyzed by HPLC with UV detection (243 nm). The HPLC separation was performed on a ODS column with acetonitrile-water (50:50) as the mobile phase. Recoveries of dymron from several agricultural products fortified at the level of 0.10 ppm were in the range of 93.3 similar to 105.2%. The limit of detection was 0.005 ppm in samples.
引用
收藏
页码：233 / 240
页数：8
相关论文
共 50 条
  • [1] Determination of alanycarb in agricultural products by HPLC
    Ito, M
    Nagayama, T
    Kobayashi, M
    Hashimoto, T
    Haneishi, N
    Tamura, Y
    Tomomatsu, T
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 1998, 39 (03): : 218 - 224
  • [2] Determination of cyclosulfamuron in agricultural products by HPLC
    Ito, M
    Nagayama, T
    Takano, I
    Kobayashi, M
    Tamura, Y
    Tateishi, Y
    Kimura, N
    Kitayama, K
    Yasuda, K
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 2000, 41 (06): : 371 - 376
  • [3] Determination of methabenzthiazuron in agricultural products by HPLC
    Kobayashi, M
    Nagayama, T
    Hashimoto, T
    Haneishi, N
    Ito, M
    Tamura, Y
    Tomomatsu, T
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 1997, 38 (05): : 351 - 357
  • [4] Determination of Diphenylamine in Agricultural Products by HPLC-FL
    Aoyagi, Mitsutoshi
    Chiba, Masahiro
    Kakimoto, Youichiro
    Nemoto, Satoru
    [J]. FOOD HYGIENE AND SAFETY SCIENCE, 2016, 57 (06): : 201 - 206
  • [5] TRANSFORMATION PRODUCTS OF THE UREA HERBICIDE DYMRON IN SOILS
    UCHIYAMA, M
    [J]. JOURNAL OF PESTICIDE SCIENCE, 1984, 9 (03): : 433 - 442
  • [6] Determination of 21 pesticides in agricultural products by HPLC-photodiode array detection
    Takatsuki, S
    Nemoto, S
    Matsuda, R
    Sasaki, K
    Toyoda, M
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 1999, 40 (04): : 314 - 319
  • [7] Determination of bentazone, inabenfide and flusulfamide in agricultural products by HPLC and confirmation by LC/MS
    Yoshii, K
    Tsumura, Y
    Nakamura, Y
    Ishimitsu, S
    Tonogai, Y
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 2000, 41 (04): : 268 - 273
  • [8] Validation of an HPLC analytical method for determination of biogenic amines in agricultural products and monitoring of biogenic amines in Korean fermented agricultural products
    Yoon H.
    Park J.H.
    Choi A.
    Hwang H.-J.
    Mah J.-H.
    [J]. Toxicological Research, 2015, 31 (3) : 299 - 305
  • [9] Analysis of phenmedipham in agricultural products by HPLC
    Imazawa, T
    Iida, T
    Matsuno, N
    Kato, F
    Ito, T
    Sasaki, K
    [J]. JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 2005, 46 (06): : 277 - 281
  • [10] Determination of butocarboxim residue in agricultural products by HPLC with post-column derivatization system
    Tseng, SH
    Chang, PC
    Chou, SS
    [J]. JOURNAL OF FOOD AND DRUG ANALYSIS, 1999, 7 (04) : 269 - 277
12345