Determination of tungsten in geochemical reference material basalt Columbia River 2 by radiochemical neutron activation analysis and inductively coupled plasma mass spectrometry

被引：5

作者：

Morrison, Samuel S. ^{[1
,2
]}

Beck, Chelsie L. ^{[2
]}

Bowen, James M. ^{[2
]}

Eggemeyer, Tere A. ^{[2
]}

Hines, C. Corey ^{[3
]}

Leizers, Martin ^{[2
]}

Metz, Lori A. ^{[2
]}

Morley, Shannon M. ^{[2
]}

Restis, Kaitlyn R. ^{[3
]}

Snow, Mathew S. ^{[4
]}

Wall, Donald E. ^{[3
]}

Clark, Sue B. ^{[1
,2
]}

Seiner, Brienne N. ^{[2
]}

机构：

[1] Washington State Univ, Dept Chem, POB 644630, Pullman, WA 99164 USA

[2] Pacific Northwest Natl Lab, POB 999,902 Battelle Blvd, Richland, WA 99352 USA

[3] Washington State Univ, Nucl Radiat Ctr, Pullman, WA 99164 USA

[4] Idaho Natl Lab, POB 1625, Idaho Falls, ID 83415 USA

来源：

JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY | 2017年 / 311卷 / 01期

关键词：

W determination; Radiochemical neutron activation analysis; Inductively coupled plasma mass spectrometry; Reference material BCR-2; Anion exchange; NUCLEAR-DATA SHEETS; IRON;

D O I：

10.1007/s10967-016-5065-1

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Determination of environmental tungsten (W) is inhibited by a lack of reference materials and practical methods to remove isobaric and radiometric interferences. We present a method that evaluates the potential use of commercially available sediment, Basalt Columbia River-2 (BCR-2), as a quality control standard for W. Tungsten concentrations determined using neutron activation analysis (NAA) and mass spectrometry are in statistical agreement at the significance level alpha = 0.05 (92 +/- 4 ng g(-1) for NAA and 100 +/- 7 ng g(-1) for mass spectrometry). These results indicate that BCR-2 may be suitable as a quality control standard for future studies.

引用

页码：749 / 754

页数：6

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