Fabrication of Lead Barium Titanate Ceramics via Conventional Solid-State Mixed Oxide Technique

(Pb0.925Ba0.075)TiO3 (PBT) ceramics have been prepared using a mixed oxide technique. The phase formation and morphology were Studied in detail via X-ray diffraction (XRD) and scanning electron microscopy (SEM). The pure tetragonal perovskite structure was discovered with calcination temperatures above 800 degrees C. The percentage of perovskite phase and particle size tends to increase with the increasing of calcination temperatures. The PBT ceramics sintered at various temperatures belonged to a pure tetragonal perovskite phase. The average grain sizes increased from 0.90 to 6.44 mu m with the increase of sintering temperatures from 1100 to 1200 degrees C. The highest density was obtained from the sample that sintered at 1150 and 1200 degrees C.