A comprehensive classification of solvent systems used for natural product purifications in countercurrent and centrifugal partition chromatography

被引：66

作者：

Skalicka-Wozniak, Krystyna ^{[1
]}

Garrard, Ian ^{[2
]}

机构：

[1] Med Univ Lublin, Med Plant Unit, Dept Pharmacognosy, PL-20093 Lublin, Poland

[2] Brunel Univ, Brunel Inst Bioengn, Adv Bioproc Ctr, Uxbridge UB8 3PH, Middx, England

来源：

NATURAL PRODUCT REPORTS | 2015年 / 32卷 / 11期

关键词：

COIL PLANET CENTRIFUGE; HIGH-SPEED; DYNAMIC EXTRACTION; SEPARATION; SELECTION;

D O I：

10.1039/c5np00061k

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

Using both library paper copies and modern electronic copies, every known, published, English-language journal paper that employs either countercurrent or centrifugal partition chromatography solvent systems for natural product purifications has been studied and the solvent systems classified in a comprehensive database. Papers were studied from the earliest found examples containing natural product separations in 1984 until the end of 2014. In total, 2594 solvent systems have been classified, of which 272 are gradient systems. To observe any trends or patterns in the data, the natural product solutes were divided into 21 classes and the solvent systems into 7 different types. The complete database, sorted according to natural product class, is available for download to assist separation scientists in future liquid-liquid chromatography purifications.

引用

页码：1556 / 1561

页数：6

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