Feedback system of a liquid-nitrogen-cooled double-crystal monochromator: design and performances

被引:133
|
作者
Proux, O
Nassif, V
Prat, A
Ulrich, O
Lahera, E
Biquard, X
Menthonnex, JJ
Hazemann, JL
机构
[1] Univ Grenoble 1, Lab Geophys Interne & Tectonophys, CNRS, UMR, F-38400 St Martin Dheres, France
[2] CEA Grenoble, DRFMC, SP2M, NRS, F-38054 Grenoble, France
[3] CNRS, Cristallog Lab, F-38042 Grenoble, France
关键词
double-crystal monochromator; cryogenic cooling; parallelism adjustment; X-ray absorption spectroscopy;
D O I
10.1107/S0909049505037441
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A new set-up is reported of an indirect cryogenic cooling system for a double-crystal monochromator which runs on the BM30b/FAME beamline at the ESRF (Grenoble, France). This device has been conceived to limit the vibrations on the first diffracting crystal and to maintain it at a constant temperature. These points are crucial for maximizing the beamline stability. Moreover, the relative angular position of the second crystal can be dynamically adjusted by a piezoelectric transducer coupled with a feedback system in order to always be at the maximum of the rocking curve during an X-ray absorption spectroscopy scan. The temperature is stabilized to an accuracy of 0.01 degrees, with two principal consequences. The energy resolution is close to the theoretical value [Delta E/E=5.6x10(-6) for Si(220)] and the precision of the energy positioning is extremely good even if the power load changes. A feedback mechanism allows a permanent and automatic optimization of the angle between the two crystals of the monochromator. The intensity of the monochromatic beam remains optimized (i) when the intensity of the electron beam decreases in the storage ring and (ii) during an energy scan.
引用
收藏
页码:59 / 68
页数:10
相关论文
共 50 条
  • [21] Diamond double-crystal monochromator at SPring-8
    Goto, S.
    Yamazaki, H.
    Shimizu, Y.
    Suzuki, M.
    Kawamura, N.
    Mizumaki, M.
    Yabashi, M.
    Tamasaku, K.
    Ishikawa, T.
    [J]. ADVANCES IN X-RAY/EUV OPTICS AND COMPONENTS VII, 2012, 8502
  • [22] Project of ultrahigh-vacuum double-crystal monochromator
    Ancharov, AI
    Gavrilov, NG
    Kondrat'ev, VI
    Poletaev, IV
    Sheromov, MA
    Shmakov, AN
    Tolochko, BP
    Tsukanov, VM
    Zhogin, IL
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2001, 470 (1-2): : 128 - 130
  • [23] INSTALLATION AND OPERATION OF THE LNLS DOUBLE-CRYSTAL MONOCHROMATOR AT CAMD
    SCHILLING, PJ
    MORIKAWA, E
    TOLENTINO, H
    TAMURA, E
    KURTZ, RL
    CUSATIS, C
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (02): : 2214 - 2216
  • [24] Vibrational stability of a cryocooled horizontal double-crystal monochromator
    Kristiansen, Paw
    Johansson, Ulf
    Ursby, Thomas
    Jensen, Brian Norsk
    [J]. JOURNAL OF SYNCHROTRON RADIATION, 2016, 23 : 1076 - 1081
  • [25] A LIQUID-NITROGEN-COOLED TELESCOPE FOR INFRARED ROCKET ASTRONOMY
    MCNUTT, DP
    SHIVANAN.K
    ZAJAC, BJ
    HARWIT, M
    [J]. ASTRONOMICAL JOURNAL, 1966, 71 (03): : 170 - &
  • [26] Improvement of the performance of a cryo-cooled monochromator at SSRF. Part I: Double-crystal parallelism
    Wu Jiaxing
    Gong Xuepeng
    Song Yuan
    Chen Jiahua
    Zhu Wanqian
    Fan Yichen
    Qin Hongliang
    Jin Limin
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2021, 985
  • [27] LIQUID-NITROGEN-COOLED INDUCTION HEAT SOURCE FOR VACUUM STUDIES
    PODLASEK, S
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1964, 35 (07): : 921 - &
  • [28] Design and feasibility of quick EXAFS scans for a 'broomstick' double-crystal monochromator at PLS beamline
    Lee, JM
    Sung, NE
    Park, JK
    Yoon, JG
    Kim, JH
    Choi, MH
    Lee, KB
    [J]. JOURNAL OF SYNCHROTRON RADIATION, 1998, 5 : 524 - 526
  • [29] A HIGHLY EFFICIENT DOUBLE-CRYSTAL MONOCHROMATOR FOR THERMAL-NEUTRONS
    MIKULA, P
    KULDA, J
    CHALUPA, B
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 1984, 40 : C372 - C372
  • [30] A COMPACT DOUBLE-CRYSTAL MONOCHROMATOR WITH A BROAD ENERGY-RANGE
    STAUDENMANN, JL
    DESLATTES, RD
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1994, 347 (1-3): : 352 - 355