(3S, 4S)-4-(Cyclopropylcarbonyl)-3-[(1R)-1-hydroxyethyl]azetidin-2-one

被引:2
|
作者
Wang, LJ
Zhang, ZD
Zheng, JF
Fang, H
Jin, LR [1 ]
机构
[1] Xiamen Univ, Coll Chem & Chem Engn, Dept Chem, Key Lab Chem Biol Fujian Prov, Xiamen 361005, Peoples R China
[2] Xiamen Univ, Coll Med, Dept Pharmaceut Sci, Xiamen 361005, Peoples R China
关键词
D O I
10.1107/S160053680600359X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal structure of the title compound, C9H13NO3, is stabilized by intermolecular O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen bonds, leading to a two-dimensional network extending parallel to the (001) plane. The absolute configuration has been assigned by reference to the chiral hydroxy C atom, which remains unchanged during the synthetic procedure.
引用
收藏
页码:O888 / O889
页数:2
相关论文
共 50 条
  • [31] 4-(4-Bromophenyl)-3-(2,5-dioxopyrrolidin-1-yl)-1-(4-methyloxyphenyl)azetidin-2-one
    Zhang, Ping
    Yu, Jing-Min
    Liu, Na
    Li, Yuan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O4487 - O4488
  • [33] A convenient stereoselective synthesis of (1R,2S,3R,4S)-3-(neopentyloxy)isoborneol
    Verdaguer, X
    Marchueta, I
    Tormo, J
    Moyano, A
    Pericàs, MA
    Riera, A
    HELVETICA CHIMICA ACTA, 1998, 81 (01) : 78 - 84
  • [34] Stereocontrolled Synthesis of (1R,3R,4S)- and (1S,3R,4S)-3,4-diaminocyclopentanols
    Guan, YS
    Green, MA
    Bergstrom, DE
    SYNLETT, 1999, (04) : 426 - 428
  • [35] BIOSYNTHESIS OF ARISTEROMYCIN - THE ROLE OF (1R,2R,3S,4S)-1-HYDROXYMETHYLCYCLOPENTANE-2,3,4-TRIOL
    HANRAHAN, J
    NAVRATILOVA, H
    SHOBERU, KA
    CROUT, DHG
    HUTCHINSON, DW
    ROBERTS, SM
    WELLINGTON, EMH
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1994, (24): : 3533 - 3536
  • [36] Enantioselective epoxidation of α,β-enones promoted by (1R,3S,4S)-2-azanorbornyl-3-methanol as an organocatalyst
    Lu, Jun
    Xu, Yun-He
    Liu, Feng
    Loh, Teck-Peng
    TETRAHEDRON LETTERS, 2008, 49 (41) : 6007 - 6008
  • [37] Stereoselective synthesis and absolute configuration of (1′R,3R,4R)-4-acetoxy-3-(2′,2′,2′-trifluoro-1′-hydroxyethyl)-azetidin-2-one
    Antolini, L
    Forni, A
    Davoli, P
    Moretti, I
    Prati, F
    TETRAHEDRON-ASYMMETRY, 1998, 9 (02) : 285 - 292
  • [38] 1-[3-(Morpholin-4-yl)propyl]-3-[(naphthalen-2-yl)oxy]-4-(3-nitro-phenyl)azetidin-2-one
    Atioglu, Zeliha
    Akkurt, Mehmet
    Jarrahpour, Aliasghar
    Heiran, Roghayeh
    Ozdemir, Namik
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2014, 70 : O833 - +
  • [39] Crystal structure of (3R,4S,1′′S,2′′S)-3-acetoxy-1-benzyl-4-(1′′-benzyloxy-2′′,3′′-isopropylidenedioxy-propyl)-azetidin-2-one, C25H29NO6
    Henkel, S
    Krämer, B
    Jäger, V
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1997, 212 (02): : 209 - 210
  • [40] Crystal structure of (3R,4S,1′R,1′′S,2′′R)-3-acetoxy-4-(2′′-acetoxyacetoxy-1′′,3′′-ethylidenedioxy-propyl)-1-(1′-phenylethyl)-azetidin-2-one, C22H27NO9
    Henkel, S
    Krämer, B
    Jäger, V
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 1997, 212 (02): : 211 - 212