Halo-heterocyclization of trans-5-phenyl-3-cinnamylsulfanyl[1,2,4]triazine into [1,3]thiazino[3,2-b][1,2,4]triazin-9-ium systems

被引：2

作者：

Kim, Dmitry G. ^{[1
]}

Rybakova, Anastasiya V. ^{[1
]}

Sharutin, Vladimir V. ^{[1
]}

Danilina, Elena I. ^{[1
]}

Sazhayeva, Olesya V. ^{[1
]}

机构：

[1] South Ural State Univ, Chelyabinsk 454080, Russia

来源：

MENDELEEV COMMUNICATIONS | 2019年 / 29卷 / 01期

关键词：

1,2,4-TRIAZINE DERIVATIVES;

D O I：

10.1016/j.mencom.2019.01.019

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Treatment of trans-5-phenyl-3-cinnamylsulfanyl[1,2,4]triazine with bromine or iodine in dichloromethane leads to halo-annulation onto the thiazine moiety with formation of (7r,8t)-7-halo-3,8-dipheny1-7,8-dihydro-6H-[1,3]thiazino[3,2-b][1,2,4]-triazin-9-ium salts. The product structure was confirmed by X-ray study.

引用

页码：59 / 60

页数：2

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