Halo-heterocyclization of trans-5-phenyl-3-cinnamylsulfanyl[1,2,4]triazine into [1,3]thiazino[3,2-b][1,2,4]triazin-9-ium systems

被引：2
|
作者：
Kim, Dmitry G. [1 ]
Rybakova, Anastasiya V. [1 ]
Sharutin, Vladimir V. [1 ]
Danilina, Elena I. [1 ]
Sazhayeva, Olesya V. [1 ]
机构：
[1] South Ural State Univ, Chelyabinsk 454080, Russia
来源：
MENDELEEV COMMUNICATIONS | 2019年 / 29卷 / 01期
关键词：
1,2,4-TRIAZINE DERIVATIVES;
D O I：
10.1016/j.mencom.2019.01.019
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Treatment of trans-5-phenyl-3-cinnamylsulfanyl[1,2,4]triazine with bromine or iodine in dichloromethane leads to halo-annulation onto the thiazine moiety with formation of (7r,8t)-7-halo-3,8-dipheny1-7,8-dihydro-6H-[1,3]thiazino[3,2-b][1,2,4]-triazin-9-ium salts. The product structure was confirmed by X-ray study.
引用
收藏
页码：59 / 60
页数：2
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