COMPARATIVE STUDY OF ESCHKA, INFRARED, THERMAL CONDUCTIVITY (TCD) AND ULTRAVIOLET METHODS OF TOTAL SULPHUR DETERMINATION IN SOLID FUELS
被引:3
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作者:
Tambani, Pamela Coelho
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机构:
Inst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, BrazilInst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, Brazil
Tambani, Pamela Coelho
[1
]
Dias dos Santos, Jorge Luis
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Inst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, BrazilInst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, Brazil
Dias dos Santos, Jorge Luis
[1
]
Hirayama, Danilo Eiji
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机构:
Inst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, BrazilInst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, Brazil
Hirayama, Danilo Eiji
[1
]
Mendonca, Marcelo Aparecido
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Inst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, BrazilInst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, Brazil
Mendonca, Marcelo Aparecido
[1
]
Antonoff, Heloisa Burkhardt
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Inst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, BrazilInst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, Brazil
Antonoff, Heloisa Burkhardt
[1
]
机构:
[1] Inst Pesquisas Tecnol Estado Sao Paulo SA, Lab Combustiveis & Lubrificantes, BR-05508901 Sao Paulo, Brazil
solid fuel;
total sulphur;
analytical methodologies;
D O I:
10.1590/S0100-40422013000600022
中图分类号:
O6 [化学];
学科分类号:
0703 ;
摘要:
The oxidation of sulphur compounds upon burning emits large quantities of SOx into the atmosphere. Therefore, there is growing interest in fast and accurate methods for analyzing sulphur content in fuels. The objective of this work was to compare four different methods of total sulphur determination in solid fuels. The methods used in this work were Eschka, Infrared, Thermal Conductivity Detection (TCD) and Ultraviolet Fluorescence Detection (UV). The preliminary results showed that TCD and UV methods (nonstandard methods for solid fuels) have similar precision to the infrared method (standard method) for high-sulphur coal samples.