One Step Synthesis and Characterization of Zirconia-Graphene Composites

被引：1
|
作者：
Xia, JianFei [1 ]
Wang, ZongHua [1 ]
Xia, YanZhi [1 ]
Zhang, FeiFei [1 ]
Zhu, FuQiang [1 ]
Li, YanHui [1 ]
机构：
[1] Qingdao Univ, Growing Base State Key Lab, Lab Fiber Mat & Modern Text, Qingdao, Peoples R China
来源：
ADVANCED RESEARCH ON ENVIRONMENTAL SCIENCE AND MATERIAL APPLICATION | 2012年 / 600卷
关键词：
ZrO2; graphene; composites; synthesis;
D O I：
10.4028/www.scientific.net/AMR.600.174
中图分类号：
X [环境科学、安全科学];
学科分类号：
08 ; 0830 ;
摘要：
Zirconia-graphene composite (ZrO2-G) has been successfully synthesized via decomposition of ZrOCl2 center dot 6H(2)O in a water-isopropanol system with dispersed graphene oxide (GO) utilizing Na2S as a precursor could enable the occurrence of the deposition of Zr4+ and the deoxygenation of GO at the same time. Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR) and X-ray diffraction (XRD) techniques were used to characterize the samples. It was found that graphene were fully coated with ZrO2, and the ZrO2 existing in tetragonal phase, which resulted in the formation of two-dimensional composite.
引用
收藏
页码：174 / 177
页数：4
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