A rapid and eco-friendly synthesis of novel and known benzopyrazines using silica tungstic acid (STA) as a new and recyclable catalyst

被引:50
|
作者
Khodabakhshi, Saeed [1 ]
Karami, Bahador [1 ]
机构
[1] Islamic Azad Univ, Gachsaran Branch, Dept Chem, Gachsaran, Iran
关键词
QUINOXALINE DERIVATIVES; SULFURIC-ACID; ROOM-TEMPERATURE; EFFICIENT; NANOPARTICLES; CONDENSATION;
D O I
10.1039/c2cy20227a
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A novel silica tungstic acid (STA) as a green catalyst has been prepared and employed for the solvent-free synthesis of novel benzopyrazines. Catalyst loadings as low as 2 mol% could be used leading to high yields of pure products. The STA was characterized by X-ray fluorescence (XRF), X-ray diffraction (XRD), inductively coupled plasma (ICP-OES) and Fourier transform infrared spectroscopy (FT-IR).
引用
收藏
页码:1940 / 1944
页数:5
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