SYNTHESIS, CHARACTERIZATION AND X-RAY STRUCTURE OF AN OXAZINE DERIVATIVE

被引:0
|
作者
Sheikhshoaie, Iran [1 ]
Belaj, Ferdinand [2 ]
Kamali, Ahmad [1 ]
机构
[1] Shahid Bahonar Univ Kerman, Dept Chem, Kerman, Iran
[2] Karl Franzens Univ Graz, Inst Chem, A-8010 Graz, Austria
关键词
1,2-Diphenylethanone; 1-Amino-2-propanol; Oxazine;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The 5,6-dihydro-6-methyl-2,3-diphenyl-2H-1,4-oxazine-2-ol compound (2) was prepared unambiguously by condensation of 1,2-diphenylethanone with 1-amino-2-propanol in the presence of glacial acetic acid. The product was characterized by FT-IR, (HNMR)-H-1, UV-Vis spectroscopy and X-ray crystallography. Quantum chemical calculations are used to the proposed mechanism.
引用
下载
收藏
页码:283 / 287
页数:5
相关论文
共 50 条
  • [21] X-ray molecular structure and antioxidant effect of a butylaminoestrogen derivative
    Flores, M.
    del Valle, L.
    Valente, B.
    Quintanar, L.
    Fernandez-G, J.
    Salgado, V
    de la Pena, A.
    JOURNAL OF THROMBOSIS AND HAEMOSTASIS, 2009, 7 : 924 - 924
  • [22] Selective Synthesis and X-Ray Structural Analysis of a Pyridocarbazole Derivative
    N. Sampath
    Rita Mathews
    M. N. Ponnuswamy
    Journal of Chemical Crystallography, 2010, 40 : 1094 - 1098
  • [23] Selective Synthesis and X-Ray Structural Analysis of a Pyridocarbazole Derivative
    Sampath, N.
    Mathews, Rita
    Ponnuswamy, M. N.
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2010, 40 (12) : 1094 - 1098
  • [24] Synthesis and X-ray structure of a new pyrrolo[1,2-b]pyridazine derivative
    Caira, MR
    Dumitrascu, F
    Draghici, C
    Dumitrescu, D
    Cristea, M
    MOLECULES, 2005, 10 (02): : 360 - 366
  • [25] X-ray shielding polyurethanes: Synthesis and characterization
    Kiran, S.
    Joseph, Roy
    INTERNATIONAL JOURNAL OF POLYMER ANALYSIS AND CHARACTERIZATION, 2017, 22 (02) : 125 - 138
  • [26] Synthesis and X-ray characterization of silicon clathrates
    Ramachandran, GK
    Dong, JJ
    Diefenbacher, J
    Gryko, J
    Marzke, RF
    Sankey, OF
    McMillan, PF
    JOURNAL OF SOLID STATE CHEMISTRY, 1999, 145 (02) : 716 - 730
  • [27] SYNTHESIS, CHARACTERIZATION, AND X-RAY CRYSTAL-STRUCTURE OF A TRIMETALLIC DIPORPHYRIN COMPLEX
    WOO, LK
    MAURYA, MR
    JACOBSON, RA
    RINGROSE, SL
    INORGANICA CHIMICA ACTA, 1993, 212 (1-2) : 337 - 340
  • [28] SYNTHESIS, CHARACTERIZATION, AND X-RAY STRUCTURE OF A NEW EXPANDED AROMATIC MACROCYCLE, OZAPHYRIN
    MILLER, DC
    JOHNSON, MR
    BECKER, JJ
    IBERS, JA
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1993, 206 : 269 - ORGN
  • [29] Synthesis, spectroscopic and X-ray structure characterization of ethylenediammonium chromate and ethylenediammonium dichromate
    Srinivasan, BR
    Dhuri, SN
    Näther, C
    Bensch, W
    INDIAN JOURNAL OF CHEMISTRY SECTION A-INORGANIC BIO-INORGANIC PHYSICAL THEORETICAL & ANALYTICAL CHEMISTRY, 2003, 42 (11): : 2735 - 2741
  • [30] Studies of bimetallic carboxylates: their synthesis, characterization, biological activity and X-ray structure
    Imtiaz-ud-Din
    Mazhar, M
    Khan, KM
    Mahon, MF
    Molloy, KC
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2004, 689 (05) : 899 - 908