One-step synthesis of nanocrystalline N-doped TiO2 powders and their photocatalytic activity under visible light irradiation

被引：13

作者：

Xu, Junna ^{[1
,2
]}

Liu, Qing ^{[1
,2
]}

Lin, Shufeng ^{[1
,2
]}

Cao, Wenbin ^{[1
,2
]}

机构：

[1] Univ Sci & Technol Beijing, Sch Mat Sci & Engn, Dept Inorgan Nonmetall Mat, Beijing 100083, Peoples R China

[2] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

来源：

RESEARCH ON CHEMICAL INTERMEDIATES | 2013年 / 39卷 / 04期

基金：

国家高技术研究发展计划(863计划); 中国国家自然科学基金;

关键词：

N-TiO2; Hydrothermal method; Photocatalysis; NITROGEN-CONCENTRATION DEPENDENCE; METHYLENE-BLUE; ANATASE;

D O I：

10.1007/s11164-012-0899-9

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Nanocrystalline N-doped TiO2 powders were successfully prepared by hydrothermal reaction for 2 h at low temperature (120 A degrees C) and at an applied pressure of 3 MPa. The grain size of the powders (calculated by use of Scherrer's method) ranged from 8.2 to 10.2 nm. The BET specific surface area ranged from 151.0 to 220.0 m(2)/g. A significant shift of the light absorption edge toward the visible light zone was observed in the UV-visible spectra. XPS results showed that nitrogen atoms were incorporated into the TiO2 lattice. The photocatalytic activity of the synthesized N-doped TiO2 powders was evaluated by measurement of photodegradation of methylene blue (MB) in aqueous solution under visible light irradiation. The amount of MB degraded increased with increasing illumination intensity.

引用

页码：1655 / 1664

页数：10

共 50 条

[31] N-doped SiO2/TiO2 mesoporous nanoparticles with enhanced photocatalytic activity under visible-light irradiation
Hou, Y. D.
Wang, X. C.
Wu, L.
Chen, X. F.
Ding, Z. X.
Wang, X. X.
Fu, X. Z.
[J]. CHEMOSPHERE, 2008, 72 (03) : 414 - 421
[32] COLL 282-Photocatalytic degradation of gaseous toluene over N-doped nanocrystalline TiO2 with enhanced activity under UV and visible light irradiation
Dong, Fan
Guo, Sen
Zhao, Weirong
Wu, Zhongbiao
[J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2007, 234
[33] Synthesis and characterization of N-doped TiO2 and its enhanced visible-light photocatalytic activity
Cheng, Xiuwen
Yu, Xiujuan
Xing, Zipeng
Yang, Lisha
[J]. ARABIAN JOURNAL OF CHEMISTRY, 2016, 9 : S1706 - S1711
[34] Visible light-induced photocatalytic and antibacterial activity of N-doped TiO2
Iwatsu, Misato
Kanetaka, Hiroyasu
Mokudai, Takayuki
Ogawa, Toru
Kawashita, Masakazu
Sasaki, Keiichi
[J]. JOURNAL OF BIOMEDICAL MATERIALS RESEARCH PART B-APPLIED BIOMATERIALS, 2020, 108 (02) : 451 - 459
[35] One-step solvothermal synthesis of N-doped TiO2 nanoparticles with high photocatalytic activity in the reduction of aqueous Cr(VI)
Li, Jing
Yang, Min
Jiang, Zun-Biao
[J]. CHINESE CHEMICAL LETTERS, 2014, 25 (02) : 283 - 286
[36] Synthesis, characterization and photocatalytic activity of doped TiO2 under visible light
Virkutyte, Jurate
Varma, Rajender S.
[J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2010, 240
[37] Use of Pt/N-doped mesoporous-assembled nanocrystalline TiO2 for photocatalytic H2 production under visible light irradiation
Sreethawong, Thammanoon
Laehsalee, Siriporn
Chavadej, Sumaeth
[J]. CATALYSIS COMMUNICATIONS, 2009, 10 (05) : 538 - 543
[38] Study of the photocatalytic activity of nanocrystalline S, N-codoped TiO2 thin films and powders under visible and sun light irradiation
Behpour, Mohsen
Atouf, Vajiheh
[J]. APPLIED SURFACE SCIENCE, 2012, 258 (17) : 6595 - 6601
[39] Synthesis and photocatalytic activity of N-doped TiO2/ZrO2 visible-light photocatalysts
Cha, Ji-An
An, Sang-Hun
Jang, Hee-Dong
Kim, Chan-Soo
Song, Dong-Keun
Kim, Tae-Oh
[J]. ADVANCED POWDER TECHNOLOGY, 2012, 23 (06) : 717 - 723
[40] N-doped TiO2 nanotube with visible light activity
Tokudome, H
Miyauchi, M
[J]. CHEMISTRY LETTERS, 2004, 33 (09) : 1108 - 1109

← 1 2 3 4 5 →